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Perkin Transactions 1 1972-2002 logo

Year 1992
Main Index

Issue 1


Front cover

pg X001; DOI:
10.1039/P199200FX001
PDF
Contents pages

pg P001; DOI:
10.1039/P199200FP001
PDF
Novel synthesis of perfluoroalkylated ,-unsaturated bromoalkane-carboxylates and -carbonitriles
Yanchang Shen and Ming Qi
pg 3; DOI:
10.1039/P19920000003
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Back cover

pg X003; DOI:
10.1039/P199200BX003
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Petunianines, unusual steroidal nitrogenous bases from Petunia inflata
Carl A. Elliger Rosalind Y. Wong Mabry Benson and Anthony C. Waiss Jr.
pg 5; DOI:
10.1039/P19920000005
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Back matter

pg P005; DOI:
10.1039/P199200BP005
PDF
An investigation of the retro Diels–Alder reaction as a method for the generation of diatomic sulfur
Thomas L. Gilchrist and Jane E. Wood
pg 9; DOI:
10.1039/P19920000009
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Prop-2-ynylic carbonates as a1,a2 synthons in palladium catalysed annulation reactions with bifunctional nucleophiles
Lifeng Geng and Xiyan Lu
pg 17; DOI:
10.1039/P19920000017
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Pennigritrem, a naturally-occurring penitrem A analogue with novel cyclisation in the diterpenoid moiety
Julia Penn Jeremy R. Biddle Peter G. Mantle John N. Bilton and Richard N. Sheppard
pg 23; DOI:
10.1039/P19920000023
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Stereoselective reductive hydroxymethylation of an annulated sugar derivative via radical cyclisation
Roger V. Bonnert Michael J. Davies Joshua Howarth Paul R. Jenkins and Nicholas J. Lawrence
pg 27; DOI:
10.1039/P19920000027
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Synthesis of arene oxide and trans-dihydro diol metabolites of isoquinoline
Derek R. Boyd R. Jeremy H. Davies Lynne Hamilton and John J. McCullough
pg 31; DOI:
10.1039/P19920000031
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Facilitation of diphosphate group elimination from geranyl diphosphate by magnesium ion chelation in cyclic monoterpenoid biosynthesis
Diana I. Ito Shunsuke Izumi Toshifumi Hirata and Takayuki Suga
pg 37; DOI:
10.1039/P19920000037
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Stereochemistry of some reactions of ring D of the diterpenoid aphidicolin
James R. Hanson Peter B. Hitchcock Andrew G. Jarvis Arnold H. Ratcliffe and Elsa M. Rodriguez-Perez
pg 41; DOI:
10.1039/P19920000041
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2-Chloro-4,5-dihydroimidazole. Part VII. Reactions with carbon disulfide and potassium O-alkyl dithiocarbonates. Synthesis and transformations of 2,3,7,8-tetrahydro-5H-diimidazo[2,1-b : 1,2-e][1,3,5]thiadiazine-5-thione
Franciszek Sczewski and Maria Gdaniec
pg 47; DOI:
10.1039/P19920000047
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Preparation of novel N-substituted phospholipids via phosphoramidite intermediates
Christopher McGuigan and Bernadette Swords
pg 51; DOI:
10.1039/P19920000051
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Synthesis of the unique all-cis cyclopentanetetraol moiety in funiculosin
Michael J. Begley John P. Madeley Gerald Pattenden and Graham F. Smith
pg 57; DOI:
10.1039/P19920000057
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Lithiation of 4-methoxy-2-pyridones. Synthetic entry to tenellin and funiculosin, and related natural 3,5-disubstituted 4-oxy-2-pyridones
Judith Buck J. Paul Madeley and Gerald Pattenden
pg 67; DOI:
10.1039/P19920000067
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Neighbouring group participation in the cleavage of steroidal -hydroxyacetals
Andrew W. Bridge George A. Morrison and Nicholas F. Wooster
pg 75; DOI:
10.1039/P19920000075
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Synthesis of medium ring ethers. Part 2. Synthesis of the fully saturated carbon skeleton of Laurencia non-terpenoid ether metabolites containing seven-, eight- and nine-membered rings
Robert W. Carling J. Stephen Clark and Andrew B. Holmes
pg 83; DOI:
10.1039/P19920000083
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Synthesis of medium ring ethers. Part 3. Disproof of the proposed 2,8-disubstituted oxocane structure for gloeosporone. Synthesis of pseudo-gloeosporone
Robert W. Carling J. Stephen Clark Andrew B. Holmes and Dirk Sartor
pg 95; DOI:
10.1039/P19920000095
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Biosynthesis of the antibiotic obafluorin from D-[U-13C]glucose and p-aminophenylalanine in Pseudomonas fluorescens
Richard B. Herbert and Andrew R. Knaggs
pg 103; DOI:
10.1039/P19920000103
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Biosynthesis of the antibiotic obafluorin from p-aminophenylalanine and glycine (glyoxylate)
Richard B. Herbert and Andrew R. Knaggs
pg 109; DOI:
10.1039/P19920000109
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Photoinduced molecular transformations. Part 127. A new [2 + 2] photoaddition of 2-amino-1,4-naphthoquinone with vinylarenes and the synthesis of 2,3-dihydronaphtho[1,2-b]furan-4,5-diones and 2,3-dihydronaphtho[2,3-b]furan-4,9-diones by -scission of alkoxyl radicals generated from the resulting photoadducts
Kazuhiro Kobayashi Akiyoshi Sasaki Hiroyasu Takeuchi and Hiroshi Suginome
pg 115; DOI:
10.1039/P19920000115
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Application of the Suzuki biphenyl synthesis to the natural products biphenomycin and vancomycin
Allan G. Brown Michael J. Crimmin and Peter D. Edwards
pg 123; DOI:
10.1039/P19920000123
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Tricarbonylchromium complexes of 2-aminotetralin derivatives. Part 2. Regio- and stereo-selective reactions
Marie Persson and Uli Hacksell
pg 131; DOI:
10.1039/P19920000131
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Chemoselective enzymatic hydrolysis of aliphatic and alicyclic nitriles
Anna de Raadt Norbert Klempier Kurt Faber and Herfried Griengl
pg 137; DOI:
10.1039/P19920000137
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syn-Selective aldol reaction of propynal–hexacarbonylcobalt complexes with ketene silyl acetals
Chisato Mukai Kimimasa Suzuki Kazuyoshi Nagami and Miyoji Hanaoka
pg 141; DOI:
10.1039/P19920000141
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1,2,3-Triazolium-1-oxide, -1-imide and 1-methanide hetero-1,3,5-triene equilibrium: ab initio calculations. A new base induced ring expansion of 1-alkyl-1,2,3-triazolium salts to 2,3-dihydro-1,2,4-triazines and 1-amino-imidazoles via the 1,2,5-triazahexa-1,3,5-triene system. Azolium 1,3-dipoles
Richard N. Butler J. Paul Duffy Desmond Cunningham Patrick McArdle and Luke A. Burke
pg 147; DOI:
10.1039/P19920000147
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Highly selective monoetherification of symmetrical diols catalysed by metallic sulfate supported on silica gel
Takeshi Nishiguchi Katsumi Kawamine and Tomoko Ohtsuka
pg 153; DOI:
10.1039/P19920000153
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Dehydrogenation of 6-azaquinazoline derivatives. Formation of unexpected quinonediimine intermediates
Imre Huber Ferenc Fülöp János Lázár Gábor Bernáth and Gábor Tóth
pg 157; DOI:
10.1039/P19920000157
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Steric and electronic effects on the photochemical reactivity of oxime acetates of ,-unsaturated aldehydes
Diego Armesto William M. Horspool Mar G. Gallego and Antonia R. Agarrabeitia
pg 163; DOI:
10.1039/P19920000163
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Reaction of anions from monoimines of benzil with alkylating agents. Photochemical reactivity of some 4-alkoxy-2-aza-1,3-dienes
Diego Armesto William M. Horspool Maria J. Ortiz and Santiago Romano
pg 171; DOI:
10.1039/P19920000171
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Instructions for authors (1992)

pg va; DOI:
10.1039/P199200000va
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IUPAC publications on nomenclature and symbolism

pg xx; DOI:
10.1039/P199200000xx
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Issue 2


Front cover

pg X005; DOI:
10.1039/P199200FX005
PDF
Back cover

pg X007; DOI:
10.1039/P199200BX007
PDF
Contents pages

pg P011; DOI:
10.1039/P199200FP011
PDF
1,2-, 1,3- and 1,4-Photocycloaddition modes on the naphthalene ring
Nataa Zupani and Boris ket
pg 179; DOI:
10.1039/P19920000179
PDF
Intramolecular cycloaddition–elimination reactions of 4-methyl-5-(substituted)-imino-2-1,2,3,4-thiatriazolines
Gerrit L'abbé and Stefan Leurs
pg 181; DOI:
10.1039/P19920000181
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A new synthetic route to furofuranoid lignans via the intramolecular Mukaiyama reaction
David R. Stevens Clive P. Till and Donald A. Whiting
pg 185; DOI:
10.1039/P19920000185
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Macrocyclic thia-alkenolides formed by intramolecular ene reactions of thioaldehydes
Samuel S.-M. Choi Gordon W. Kirby and Mohinder P. Mahajan
pg 191; DOI:
10.1039/P19920000191
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2,4-Bisimino-1,3-diazetidines: iminophosphoranes, carbodiimides and related betaines
Pedro Molina Mateo Alajarin Carmen Lopez-Leonardo Felix Hernandez Cano Antonio L. Llamas-Saiz Concepcion Foces-Foces Rosa Maria Claramunt and Jose Elguero
pg 199; DOI:
10.1039/P19920000199
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A new and unequivocal method for establishing the position of N-glycosylation of unsymmetrically C-substituted imidazoles
Timothy J. Benson and Brian Robinson
pg 211; DOI:
10.1039/P19920000211
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Azoles. Part 8. Metallation and bromine lithium exchange reactions of polyhalogenothiazoles
Salah Athmani Andrew Bruce and Brian Iddon
pg 215; DOI:
10.1039/P19920000215
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Enantioselective construction of quaternary stereogenic centres possessing a fluorine atom
Masataka Ihara Nobuaki Taniguchi Tomoko Kai Ken Satoh and Keiichiro Fukumoto
pg 221; DOI:
10.1039/P19920000221
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Spiroannulation by the [2,3]sigmatropic rearrangement via the cyclic allylsulfonium ylide. A stereoselective synthesis of (+)-acorenone B
Fusao Kido Toshiya Abiko and Michiharu Kato
pg 229; DOI:
10.1039/P19920000229
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Conversion of 2-acetamido-2-deoxy--D-glucopyranose (N-acetylglucosamine) into 2-acetamido-2-deoxy--D-galactopyranose (N-acetylgalactosamine) using a biotransformation to generate a selectively deprotected substrate for SN2 inversion
David Chaplin David H. G. Crout Stephen Bornemann David W. Hutchinson and Riaz Khan
pg 235; DOI:
10.1039/P19920000235
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Tricyclic heteroaromatic systems containing a bridgehead nitrogen atom. Part 3. [1,2,4]Triazolo[3,4 : 3,2]pyrazolo[3,4-d]pyrimidines, tetrazolo[1,5 : 1,5]pyrazolo[3,4-d]pyrimidines and pyrimido-[5,4 : 4,5]pyrazolo[3,2-c][1,2,4]triazines
Julian M. C. Golec Richard M. Scrowston and Michael Dunleavy
pg 239; DOI:
10.1039/P19920000239
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Direct synthesis of N-protected chiral amino acids from imidodicarbonates employing either Mitsunobu or triflate alkylation. Feasibility study using lactate with particular reference to 15N-labelling
Fredrik Degerbeck Bengt Fransson Leif Grehn and Ulf Ragnarsson
pg 245; DOI:
10.1039/P19920000245
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Synthesis and biological activity of 9-mercaptodethiobiotin—a putative biotin precursor in Escherichia coli
Robert L. Baxter Dominic J. Camp Andrew Coutts and Nicholas Shaw
pg 255; DOI:
10.1039/P19920000255
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Synthesis of tricarbonyl(vinylallene)iron(0) complexes from tricarbonyl(vinylketene)iron(0) complexes and their oxidation to 5,5-disubstituted furan-2(5H)-ones
Stephen P. Saberi and Susan E. Thomas
pg 259; DOI:
10.1039/P19920000259
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A new convenient synthesis of 2-trifluoromethyl substituted aspartic acid and its isopeptides. Part 11
Norbert Sewald Jürgen Riede Peter Bissinger and Klaus Burger
pg 267; DOI:
10.1039/P19920000267
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Syntheses of functionalised pyrido[2,3-b]indoles
Ian T. Forbes Christopher N. Johnson and Mervyn Thompson
pg 275; DOI:
10.1039/P19920000275
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Reactions of ethoxycarbonylmethylene(triphenyl)phosphorane with some ortho-quinones in the presence of triphenylphosphine, alcohols and acetic anhydride
Demetrios N. Nicolaides Spyros G. Adamopoulos Demetrios A. Lefkaditis Konstantinos E. Litinas and Petroula V. Tarantili
pg 283; DOI:
10.1039/P19920000283
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Acylation with 1,1,1-trifluoroacetone of the azaallyl carbanion from ethyl bis(methylthio)methyleneaminoacetate
José-Gonzalo Rodriguez Aurea Perales Carlos Alvarez Ibarra Maria I. López-Sánchez and Maria L. Quiroga
pg 291; DOI:
10.1039/P19920000291
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Synthesis of 2,4-dideoxy-4-hydroxyphosphonoyl-D-erythro- and -L-threo-pentofuranoses
Tadashi Hanaya Ayashi Noguchi Margaret-Ann Armour Alan M. Hogg and Hiroshi Yamamoto
pg 295; DOI:
10.1039/P19920000295
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Issue 3


Front cover

pg X009; DOI:
10.1039/P199200FX009
PDF
Back cover

pg X011; DOI:
10.1039/P199200BX011
PDF
Contents pages

pg P015; DOI:
10.1039/P199200FP015
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An arylhydroxylamine O-sulfonate is the probable intermediate in the peroxydisulfate oxidation of aromatic amines
Edward J. Behrman
pg 305; DOI:
10.1039/P19920000305
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Regio- and enantio-selective photodimerisation of cyclohex-2-enone as an inclusion complex with a new optically active host, (–)-1,4-bis[3-(o-chlorophenyl)-3-hydroxy-3-phenylprop-1-ynyl]benzene: preparation of the optically pure (–)-syn-trans-dimer of cyclohex-2-enone
Koichi Tanaka Osamu Kakinoki and Fumio Toda
pg 307; DOI:
10.1039/P19920000307
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A facile total synthesis of isoquinolone alkaloids
Albert W. M. Lee Wing Hong Chan and Eddy T. T. Chan
pg 309; DOI:
10.1039/P19920000309
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Acceleration of ortho ester Claisen rearrangement by a commercial microwave oven
Adusumilli Srikrishna and Sankuratri Nagaraju
pg 311; DOI:
10.1039/P19920000311
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A convenient one-pot synthesis of -fluoro-,-unsaturated nitriles from diethyl cyanofluoromethanephosphonate
Ze-Qi Xu and Darryl D. DesMarteau
pg 313; DOI:
10.1039/P19920000313
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Pig liver alcohol dehydrogenase catalysed stereoselective reduction of cage-shaped ketones. Preparation of axially chiral (–)-(R)-adamantane-2,6-diol with high enantiomeric purity
Yoshiki Hirose Munehisa Okutsu Mika Anzai Koichiro Naemura and Hiroaki Chikamatsu
pg 317; DOI:
10.1039/P19920000317
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Transition metal mediated synthesis of ()-chuangxinmycin methyl ester
Michael J. Dickens Timothy J. Mowlem David A. Widdowson Alexandra M. Z. Slawin and David J. Williams
pg 323; DOI:
10.1039/P19920000323
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Synthesis of allylstannanes and vinylstannanes by the stannyl-cupration of allenes
Asunción Barbero Purificación Cuadrado Ian Fleming Ana M. González and Francisco J. Pulido
pg 327; DOI:
10.1039/P19920000327
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Anodic cyanation of benzo[b]thiophenes
Kunihisa Yoshida and Kohji Miyoshi
pg 333; DOI:
10.1039/P19920000333
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A concise synthesis of the pseudoguaianolide skeleton
Luiz-Claudio de Almeida Barbosa and John Mann
pg 337; DOI:
10.1039/P19920000337
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Total synthesis of symbioramide, a novel Ca2+-ATPase activator from Symbiodinium sp
Jun Yoshida Masako Nakagawa Hiroko Seki and Tohru Hino
pg 343; DOI:
10.1039/P19920000343
PDF
Hetero-ring lithiation of N-methyl-4-quinolone and N-methylquinoline-4-thione
Mercedes Alvarez Marisa Salas Lluis Rigat Ana de Veciana and John A. Joule
pg 351; DOI:
10.1039/P19920000351
PDF
Enamine chemistry. Part 37. Reaction of methyl vinyl ketone with 1,8a-2-octalone dienamines. Synthesis of octahydro-1H-benzo[d]naphthalene-2,10(3H,11H)-diones and 9-acetylperhydro-2,4a-ethanonaphthalen-3-ones
Peter W. Hickmott and Richard Simpson
pg 357; DOI:
10.1039/P19920000357
PDF
Surface-mediated solid-phase reaction. Part 2. Highly selective mono- and di-C-alkylation of 1,3-dicarbonyl compounds on the surface of alumina
Brindaban C. Ranu and Sanjay Bhar
pg 365; DOI:
10.1039/P19920000365
PDF
Simple and condensed -lactams. Part 13. Synthesis of some 1-(3-acylamino-2-oxoazetidin-1-yl)-cyclopentane- and -cyclohexanecarboxylic acids
József Fetter Károly Lempert József Nagy József Nyitrai Pál Sohár Zoltán Tombor and Károly Zauer
pg 369; DOI:
10.1039/P19920000369
PDF
Electrochemical studies on haloamides. Part 3. Haloacetamides and halo-acetohydroxamates
Maria Antonietta Casadei Barbara Di Rienzo Achille Inesi and Franco Micheletti Moracci
pg 375; DOI:
10.1039/P19920000375
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Electrochemical studies on haloamides. Part 4. Reactivity of haloacetamides and haloacetohydroxamates toward electrogenerated diethyl malonate anion
Maria Antonietta Casadei Barbara Di Rienzo Achille Inesi and Franco Micheletti Moracci
pg 379; DOI:
10.1039/P19920000379
PDF
New macrocycles of carbon, nitrogen and sulfur atoms incorporating 4,5-dithio-1,3-dithiole-2-thione units
Berhane Girmay Allan E. Underhill Jeremy D. Kilburn Thomas K. Hansen Jan Becher Karithath S. Varma and Peter Roepstorff
pg 383; DOI:
10.1039/P19920000383
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Lewis acid catalysed Michael-type addition. A new regio- and diastereo-selective annulation method using methyl vinyl ketone
Pierre Duhamel Gilles Dujardin Laurent Hennequin and Jean-Marie Poirier
pg 387; DOI:
10.1039/P19920000387
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Corrigendum
P. M. Burden H. R. Capper R. D. Allan and G. A. R. Johnston
pg 397; DOI:
10.1039/P19920000397
PDF
Conference diary

pg 399; DOI:
10.1039/P19920000399
PDF

Issue 4


Front cover

pg X013; DOI:
10.1039/P199200FX013
PDF
Back cover

pg X015; DOI:
10.1039/P199200BX015
PDF
Contents pages

pg P019; DOI:
10.1039/P199200FP019
PDF
A new method for the dehydration of -hydroxy sulfones: synthesis of (E,S)--hydroxy-,-unsaturated sulfones and (S)-?-hydroxy-(E,E)-,-dienyl sulfones
Suk-Ku Kang Young-Won Park Sung-Gyu Kim and Jae-Hoon Jeon
pg 405; DOI:
10.1039/P19920000405
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A superior synthesis of diaryl ethers by the use of ultrasound in the Ullmann reaction
Keith Smith and Dennis Jones
pg 407; DOI:
10.1039/P19920000407
PDF
Partial reduction of diazines
James R. Russell C. David Garner and John A. Joule
pg 409; DOI:
10.1039/P19920000409
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Syntheses of pyrido[2,3-a]phenothiazine-type near-IR colour formers
Yuji Kubo Hiroshi Yasuoka Shin-ichi Hamaguchi and Katsuhira Yoshida
pg 411; DOI:
10.1039/P19920000411
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Diels–Alder reactions of pyrano[3,4-b]indol-3-ones and a 2-benzopyran-3-one with hetero substituted olefins: generation of carbazole and naphthalene derivatives by elimination instead of dehydrogenation
Peter I. Van Broeck Philippe E. Van Doren Suzanne M. Toppet and Georges J. Hoornaert
pg 415; DOI:
10.1039/P19920000415
PDF
Regiospecific synthesis of 2-fluoro-3-O-methylestrone using caesium fluorosulfate
Louis J. Diorazio David A. Widdowson and John M. Clough
pg 421; DOI:
10.1039/P19920000421
PDF
Photoinduced molecular transformations. Part 130. Novel stereospecific photorearrangement and stereospecific addition of methanol in steroidal ,-unsaturated cyclic ketone oximes
Hiroshi Suginome Makoto Kaji Toshiharu Ohtsuka Shinji Yamada Takashi Ohki Hisanori Senboku and Akio Furusaki
pg 427; DOI:
10.1039/P19920000427
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Electrophile-mediated cyclisations involving the allene -system. Stereoselectivity and synthetic utility of PdII-catalysed heteroatom cyclisation reactions. X-Ray molecular structure of methyl 2-[trans-3-phenyl-N-(p-tolylsulfonyl)pyrrolidin-2-yl]acrylate
Timothy Gallagher Ian W. Davies Stephen W. Jones David Lathbury Mary F. Mahon Kieran C. Molloy Robert W. Shaw and Peter Vernon
pg 433; DOI:
10.1039/P19920000433
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Some reactions of (5R)-2-methylene-5-(thymin-1-yl)-2,5-dihydrofuran
Bhalchandra V. Joshi and Colin B. Reese
pg 441; DOI:
10.1039/P19920000441
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Azepinones. Part 1. Synthesis of 1,2,3,7-tetrahydroazepin-4-ones and hexahydroazepin-3-ones
Fiona A. Fraser George R. Proctor and James Redpath
pg 445; DOI:
10.1039/P19920000445
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Umpolung of reactivity at the C-5 position of uracil: 1,2 facile nucleophilic reactions of thiolate ions at C-5 of 6-cyano-1,3-dimethyluracil to procure 5-alkyl or 5-aryl-thio-1,3-dimethyluracils
Subodh Kumar and Swapandeep Singh Chimni
pg 449; DOI:
10.1039/P19920000449
PDF
ZnII-promoted D-homorearrangement of 17-hydroxy-3-methoxyandrost-5-ene-17-carbaldehyde
Laura Schor Eduardo G. Gros and Alicia M. Seldes
pg 453; DOI:
10.1039/P19920000453
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New antitumour bicyclic hexapeptides, RA-IX and -X from Rubia cordifolia. Part 3. Conformation–antitumour activity relationship
Hideji Itokawa Tetsuo Yamamiya Hiroshi Morita and Koichi Takeya
pg 455; DOI:
10.1039/P19920000455
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Electrophilic substitution in indoles. Part 18. Cyclisation of N-acyltryptamines
Kshetra M. Biswas the late Anthony H. Jackson Mozaina M. Kobaisy and Patrick V. R. Shannon
pg 461; DOI:
10.1039/P19920000461
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General method for the synthesis of 2-azido-2,3-dideoxynucleosides by the use of [1,2]-hydride shift and -elimination reactions
Masajiro Kawana and Hiroyoshi Kuzuhara
pg 469; DOI:
10.1039/P19920000469
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Novel quasiphosphonium ylides from the reaction of trialkyl phosphites with dialkyl benzoylphosphonates: evidence for carbene intermediates in the intramolecular cyclisation of 2-substituted dialkyl benzoylphosphonates
D. Vaughan Griffiths Penelope A. Griffiths Belinda J. Whitehead and John C. Tebby
pg 479; DOI:
10.1039/P19920000479
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Photoaddition of ethenes to 1,4-naphthoquinone: factors influencing the site of reaction
Derek Bryce-Smith Elizabeth H. Evans Andrew Gilbert and Hilary S. McNeill
pg 485; DOI:
10.1039/P19920000485
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Biotransformations using clostridia: stereospecific reductions of a -keto ester
Markus Christen David H. G. Crout Robert A. Holt J. Gareth Morris and Helmut Simon
pg 491; DOI:
10.1039/P19920000491
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A novel chiral approach to trans-3a,4,5,9b-tetrahydro-1H-benz[e]indene
Hideo Nemoto Norikazu Matsuhashi Atsushi Satoh and Keiichiro Fukumoto
pg 495; DOI:
10.1039/P19920000495
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Preparation of benzocyclobutenones via the photochemical cyclization of 1-(ortho-alkylaryl)-2,2,4-trimethylpentane-1,3-diones
Michikazu Yoshioka Shinobu Momose Kaori Nishizawa and Tadashi Hasegawa
pg 499; DOI:
10.1039/P19920000499
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Synthesis of cyclic and acyclic oligocytidylates by uranyl ion catalyst in aqueous solution
Hiroaki Sawai Katsutaka Higa and Kensei Kuroda
pg 505; DOI:
10.1039/P19920000505
PDF
Heterocycles in asymmetric synthesis. Part 1. Construction of the chiral building blocks for enantioselective alkaloid synthesis via an asymmetric intramolecular Michael reaction
Yoshiro Hirai Takashi Terada Takao Yamazaki and Takefumi Momose
pg 509; DOI:
10.1039/P19920000509
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Heterocycles in asymmetric synthesis. Part 2. Efficient asymmetric approaches to heteroyohimbine, yohimbine and related alkaloids
Yoshiro Hirai Takashi Terada Takao Yamazaki and Takefumi Momose
pg 517; DOI:
10.1039/P19920000517
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Conference diary

pg 525; DOI:
10.1039/P19920000525
PDF

Issue 5


Front cover

pg X017; DOI:
10.1039/P199200FX017
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Back cover

pg X019; DOI:
10.1039/P199200BX019
PDF
Contents pages

pg P023; DOI:
10.1039/P199200FP023
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Back matter

pg P027; DOI:
10.1039/P199200BP027
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Synthesis of ()-aphanorphine via an aminylium ion intermediate
Toshio Honda Atsunori Yamamoto Yingshe Cui and Masayoshi Tsubuki
pg 531; DOI:
10.1039/P19920000531
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Remote control of double bond stereochemistry in the Wadsworth–Emmons reaction
Pedro L. López Tudanca Keith Jones and Peter Brownbridge
pg 533; DOI:
10.1039/P19920000533
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A tandem silica-induced ring-opening and cyclisation of 1-aryl-1-chlorocyclopropanes leading to indenes
Mark S. Baird Richard Dacre and Jeremy Tomkinson
pg 535; DOI:
10.1039/P19920000535
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Novel and efficient synthesis of rotenoids via intramolecular radical arylation
S. Asiah Ahmad-Junan Peter C. Amos and Donald A. Whiting
pg 539; DOI:
10.1039/P19920000539
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Tandem Michael addition–[3,3]sigmatropic rearrangement processes. Part 2. Construction of cyclopropa[3,4]pyrrolo[3,2-e]indol-4-one (CPI) unit of antitumour antibiotic CC-1065
Masahiro Toyota and Keiichiro Fukumoto
pg 547; DOI:
10.1039/P19920000547
PDF
Total synthesis of (–)--kainic acid
Jeremy Cooper David W. Knight and Peter T. Gallagher
pg 553; DOI:
10.1039/P19920000553
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Synthesis and characterisation of unusual tetraaminoalkenes (enetetramines)
Engin Cetinkaya Peter B. Hitchcock Hatam A. Jasim Michael F. Lappert and Kostas Spyropoulos
pg 561; DOI:
10.1039/P19920000561
PDF
Biosynthesis of the 24-methylcholesterols dihydrobrassicasterol and campesterol in cultured cells of Amsonia elliptica: incorporation of [1,2-13C2]acetate and [2-13C,2H3]acetate
Shujiro Seo Atsuko Uomori Yohko Yoshimura (the late) Ken'ichi Takeda Hiroshi Noguchi Yutaka Ebizuka Ushio Sankawa and Haruo Seto
pg 569; DOI:
10.1039/P19920000569
PDF
Studies of chromenes. Part 10. Oxiranes of nitrochromenes
Philip E. Brown and Robert A. Lewis
pg 573; DOI:
10.1039/P19920000573
PDF
Synthesis of a pyranonaphthoquinone-spiroacetal
Margaret A. Brimble and Michael R. Nairn
pg 579; DOI:
10.1039/P19920000579
PDF
Synthesis of 6-hydroximino-3-oxo steroids, a new class of aromatase inhibitor
Herbert L. Holland Sudalaiyandi Kumaresan Liat Tan and Vincent C. O. Njar
pg 585; DOI:
10.1039/P19920000585
PDF
Potential use of carbocyclic nucleosides for the treatment of AIDS: chemo-enzymatic syntheses of the enantiomers of carbovir
Chris T. Evans Stanley M. Roberts Karoline A. Shoberu and Alan G. Sutherland
pg 589; DOI:
10.1039/P19920000589
PDF
Parquin and carboxyparquin, toxic kaurene glycosides from the shrub Cestrum parqui
Clive M. Pearce Nicholas J. Skelton Stephen Naylor Rajamoorthi Kanaan Janice Kelland Peter B. Oelrichs Jeremy K. M. Sanders and Dudley H. Williams
pg 593; DOI:
10.1039/P19920000593
PDF
Viologen-mediated reductive desulfonylation of -nitro sulfones by sodium dithionite
Kwanghee Koh Park Chul Woo Lee and Sook Young Choi
pg 601; DOI:
10.1039/P19920000601
PDF
Simple synthesis of hexahydrocannabinoids using phenylboric acid catalyst
William S. Mufphy Sudersan M. Tuladhar and Brian Duffy
pg 605; DOI:
10.1039/P19920000605
PDF
Electron acceptor molecules: new, expedient synthesis of substituted 7,7,8,8-tetracyano-p-quinodimethane (TCNQ) derivatives and the X-ray crystal structure of 2,5-dibromo-TCNQ
Martin R. Bryce Andrew M. Grainger Masihul Hasan Geoffrey J. Ashwell Paul A. Bates and Michael B. Hursthouse
pg 611; DOI:
10.1039/P19920000611
PDF
Secondary mould metabolites. Part 36. Isolation and structure elucidation of sulcatines C–E, novel norsesquiterpenes from Laurilia sulcata, and 7-epi-sulcatine D
Alberto Arnohe Gianluca Nasini Orso Vajna de Pava and Gemma Assante
pg 615; DOI:
10.1039/P19920000615
PDF
Synthesis of 1,3-thiazetidines and 2,1,4-oxathiazolidines by high yielding novel photochemical rearrangements
Nigel K. Capps Gareth M. Davies Peter B. Hitchcock David Loakes Richard W. McCabe and Douglas W. Young
pg 621; DOI:
10.1039/P19920000621
PDF
Photolytic and chromium(II)-promoted addition reactions of N-halogenoformamides with alkenes
André Goosen Cedric W. McCleland and Alan J. Merrifield
pg 627; DOI:
10.1039/P19920000627
PDF
Stereospecific synthesis of the 2,3-trans-3,4-cis trisubstituted tetrahydrofuran lignan ()-dihydrosesamin
David R. Stevens and Donald A. Whiting
pg 633; DOI:
10.1039/P19920000633
PDF
-L-Glutamyl-O-acyl-L-serylglycine derivatives: synthesis, purification and evaluation as inhibitors of glyoxalases
Theodore W. C. Lo and Paul J. Thornalley
pg 639; DOI:
10.1039/P19920000639
PDF
Brombyin-I [(rel)- 4-acetyl-3-(1,3-benzodioxol-5-yl)-1,4,4a,5,6,7,8,8a-octahydronaphthalen-1-ol] and brombyin-II [(rel)-4-acetyl-3-(1,3-benzodioxol-5-yl)-3,4,4a,5,6,7,8,8a-octahydronaphthalene]: a novel type of natural product isolated from the stem bark of Brombya platynema. F. Muell
Ian C. Parsons Alexander I. Gray Thomas G. Hartley Brian W. Skelton Peter G. Waterman and Allan H. White
pg 645; DOI:
10.1039/P19920000645
PDF
Conference diary

pg 651; DOI:
10.1039/P19920000651
PDF

Issue 6


Front cover

pg X021; DOI:
10.1039/P199200FX021
PDF
Back cover

pg X023; DOI:
10.1039/P199200BX023
PDF
Contents pages

pg P029; DOI:
10.1039/P199200FP029
PDF
Back matter

pg P033; DOI:
10.1039/P199200BP033
PDF
A synthesis of 2,6-dideoxy-2-fluoro-L-glycopyranose from D-fructose: synthesis of 1,3,4-tri-O-acetyl-2,6-dideoxy-2-fluoro-L-talopyranose
Yasushi Takagi Geun-Jho Lim Tsutomu Tsuchiya and Sumio Umezawa
pg 657; DOI:
10.1039/P19920000657
PDF
Control of the enantioselectivity of the bioreduction with immobilized bakers' yeast in a hexane solvent system
Yoshinobu Naoshima Jusei Maeda and Yoshihito Munakata
pg 659; DOI:
10.1039/P19920000659
PDF
Regioselective enzymatic acetylation of methyl 4,6-O-benzylidene-- and -D-glucopyranoside
Matthew J. Chinn Gilles Lacazio David G. Spackman Nicholas J. Turner and Stanley M. Roberts
pg 661; DOI:
10.1039/P19920000661
PDF
Ophiorrhizine, a new quaternary indole alkaloid related to cinchonamine, from Ophiorrhiza major Ridl.
Dayar Arbain Lindsay T. Byrne Deddi Prima Putra Melvyn V. Sargent Brian W. Skelton and Allan H. White
pg 663; DOI:
10.1039/P19920000663
PDF
A new glucoalkaloid from Uncaria glabrata
Dayar Arbain Lindsay T. Byrne Magda Mina Putra Melvyn V. Sargent and Mardius Syarif
pg 665; DOI:
10.1039/P19920000665
PDF
Facile enzymatic synthesis of N-acyl-enkephalin amides
Iqbal Gill and Evgeny N. Vulfson
pg 667; DOI:
10.1039/P19920000667
PDF
Synthesis and spectral characterization of tricarbonylchromium complexes of calix[4]arene conformers
Hideshi Iki Taketoshi Kikuchi and Seiji Shinkai
pg 669; DOI:
10.1039/P19920000669
PDF
A new approach to the synthesis of peltogynoids, natural isochromeno[4,3-b]-chromenes
S. Asiah Ahmad-Junan and Donald A. Whiting
pg 675; DOI:
10.1039/P19920000675
PDF
Total synthesis of heptacyclic Aspidosperma alkaloids. Part 3. Synthesis of an advanced intermediate in the synthesis of alalakine
Abdelhamid Belattar and J. Edwin Saxton
pg 679; DOI:
10.1039/P19920000679
PDF
2H-benzimidazoles (isobenzimidazoles). Part 6. Sulfur derivatives
Justine C. Hazelton Brian Iddon Hans Suschitzky and Ley H. Woolley
pg 685; DOI:
10.1039/P19920000685
PDF
High diastereoselection in the aldol reaction of the bistrimethylsilyl enol ether of methyl acetoacetate with 2-benzyloxyhexanal: synthesis of (–)-pestalotin
Hisahiro Hagiwara Katsuhiko Kimura and Hisashi Uda
pg 693; DOI:
10.1039/P19920000693
PDF
Oxazol-5(4H)-ones. Part 7. New synthesis of oxazolo[5,4-b]pyridines
M. Luisa Gelmi Donate Pocar Monica Viziano Riccardo Destro and Felicita Merati
pg 701; DOI:
10.1039/P19920000701
PDF
Hypervalent iodine in the synthesis of bridgehead heterocycles: novel and facile syntheses of 3-substituted-5,6-dihydroimidazo[2,1-b]thiazoles and 3-phenylthiazolo[3,2-a]benzimidazole from acetophenones using [hydroxy(tosyloxy)iodo]benzene
Om Prakash Neena Rani and Seema Goyal
pg 707; DOI:
10.1039/P19920000707
PDF
Enantioselective synthesis of -hydroxy esters by indium-induced Reformatsky reaction
Perminder S. Johar Shuki Araki and Yasuo Butsugan
pg 711; DOI:
10.1039/P19920000711
PDF
Base-promoted eliminations within halogenated [n.m.1]propellene frameworks
Martin G. Banwell Brian Halton Trevor W. Hambley Neil K. Ireland Con Papamihail Sarah G. G. Russell and Michael R. Snow
pg 715; DOI:
10.1039/P19920000715
PDF
Photochromic heterocyclic fulgides. Part 6. Base-catalysed cyclizations of 1-(2,5-dimethyl-3-furyl and 2,5-dimethyl-3-thienyl)ethylidene(isopropylidene)succinic anhydrides and related compounds
Sean L. Bowden Stuart A. Harris Harry G. Heller and Michael J. E. Hewlins
pg 725; DOI:
10.1039/P19920000725
PDF
Synthesis and some properties of D-myo-inositol 1,4,5-tris(dihydrogen phosphate)
Shoichiro Ozaki Yoshihisa Kondo Naokazu Shiotani Tomio Ogasawara and Yutaka Watanabe
pg 729; DOI:
10.1039/P19920000729
PDF
Corrigendum
Derrick L. J. Clive Ahmad Khodabocus Peter G. Vernon A. Gaëtan Angoh Luc Bordeleau Donald S. Middleton Christopher Lowe and Dorit Kellner
pg 739; DOI:
10.1039/P19920000739
PDF
Conference diary

pg 741; DOI:
10.1039/P19920000741
PDF

Issue 7


Front cover

pg X025; DOI:
10.1039/P199200FX025
PDF
Back cover

pg X027; DOI:
10.1039/P199200BX027
PDF
Contents pages

pg P035; DOI:
10.1039/P199200FP035
PDF
Allene synthesis via boron-stabilised alkenyl carbanions
Andrew Pelter Keith Smith and Kevin D. Jones
pg 747; DOI:
10.1039/P19920000747
PDF
Formation of a 12-aza steroid by 1 -aza triene cyclisation
Thomas L. Gilchrist and Maureen A. M. Healy
pg 749; DOI:
10.1039/P19920000749
PDF
Unusual oxidation in thionyl chloride: novel synthesis of methyl 3-alkoxy-1,4-dioxo-1,2,3,4-tetrahydroisoquinoline-3-carboxylates
John F. Beattie and Neil J. Hales
pg 751; DOI:
10.1039/P19920000751
PDF
Synthesis and absorption/emission spectroscopic properties of bis(phenylethynyl)benzenes and 9,10-bis(phenylethynyl)anthracenes
Shin'ichi Nakatsuji Kosei Matsuda Yukiko Uesugi Kenichiro Nakashima Shuzo Akiyama and Walter Fabian
pg 755; DOI:
10.1039/P19920000755
PDF
Sodium hydride as a nucleophilic agent. Part 1. A new synthesis of 2,3-biquinolyls
Alexander V. Aksenov Igor V. Magedov and Yuri I. Smushkevich
pg 759; DOI:
10.1039/P19920000759
PDF
Photochemical transformations of cephalosporins
Nigel K. Capps Gareth M. Davies Peter B. Hitchcock and Douglas W. Young
pg 763; DOI:
10.1039/P19920000763
PDF
Novel redox cyclisation products derived from 2-acylpyrroles and trans-3-bromo-3,4-dihydro-4-hydroxy-2,2-dimethyl-2H-chromene-6-carbonitrile
Derek R. Buckle Susan C. Connor Drake S. Eggleston Andrew Faller Ivan L. Pinto Simon A. Readshaw and David G. Smith
pg 769; DOI:
10.1039/P19920000769
PDF
Preparation, isolation and X-ray crystallographic structure determination of a stable, crystalline carbonic anhydride of an N-protected -amino acid
Chat-On Chan Christopher J. Cooksey and David Crich
pg 777; DOI:
10.1039/P19920000777
PDF
Biologically active clerodane-type diterpene alcohol and its glycosides from the root-stalks of ferns
Hamid Latif Siddiqui Kiyotaka Munesada and Takayuki Suga
pg 781; DOI:
10.1039/P19920000781
PDF
An efficient route to the tropane alkaloids
John Mann and Luiz-Claudio de Almeida Barbosa
pg 787; DOI:
10.1039/P19920000787
PDF
C-nucleosides. Part 18. Stereoselective annulation of 6-acetoxy-6-(2,3,5-tri-O-benzoyl--D-ribofuranosyl)pyran-3(2H,6H)-one with ethylene glycol to pyrano-[2,3-b]-1,4-dioxine glycosides
Noriaki Morishita Shiho Honmi Chihiro Ito and Isamu Maeba
pg 791; DOI:
10.1039/P19920000791
PDF
Synthesis of 3,4-bridged indoles by photocyclisation reactions. Part 1. Photocyclisation of halogenoacetyl tryptophan derivatives
Anthony L. Beck Mark Mascal Christopher J. Moody Alexandra M. Z. Slawin David J. Williams and William J. Coates
pg 797; DOI:
10.1039/P19920000797
PDF
Synthesis of 3,4-bridged indoles by photocyclisation reactions. Part 2. Photocyclisation of halogenoacetyl tryptophol derivatives and -chloro indol-3-ylalkanoate esters
Anthony L. Beck Mark Mascal Christopher J. Moody and William J. Coates
pg 813; DOI:
10.1039/P19920000813
PDF
Synthesis of (–)-indolactam V
Mark Mascal Christopher J. Moody Alexandra M. Z. Slawin and David J. Williams
pg 823; DOI:
10.1039/P19920000823
PDF
Beckmann rearrangements in bicyclo[2.2.1]heptan-2-one oximes
Peter A. Hunt Christopher J. Moody Alexandra M. Z. Slawin David J. Williams Peter L. Myers and Colin Smith
pg 831; DOI:
10.1039/P19920000831
PDF
Biosynthesis of the A/B/C/D-ring system of the rotenoid amorphigenin by Amorpha fruticosa seedlings
Prabha Bhandari Leslie Crombie Peter Daniels Ian Holden Nicholas Van Bruggen and Donald A. Whiting
pg 839; DOI:
10.1039/P19920000839
PDF
Biosynthesis of rotenone and amorphigenin. Study of the origins of isopropenyl-substituted dihydrofuran E-rings using isotopically labelled late precursors
Prabha Bhandari Leslie Crombie Geoffrey W. Kilbee Stephen J. Pegg Geoffrey Proudfoot John Rossiter Mark Sanders and Donald A. Whiting
pg 851; DOI:
10.1039/P19920000851
PDF
Stereoselective construction of cis-transoid-cis-tricyclo[7.3.0.0]dodecanes by an intramolecular Diels–Alder reaction: a formal total synthesis of ()-9(12)-capnellene
Masataka Ihara Takayuki Suzuki Mamoru Katogi Nobuaki Taniguchi and Keiichiro Fukumoto
pg 865; DOI:
10.1039/P19920000865
PDF
Isolation and structural elucidation of syringostatins, phytotoxins produced by Pseudomonas syringae pv. syringae lilac isolate
Naoyuki Fukuchi Akira Isogai Jiro Nakayama Seiji Takayama Shuichi Yamashita Kazuo Suyama and Akinori Suzuki
pg 875; DOI:
10.1039/P19920000875
PDF
Biscyclophanes. Part 1: synthesis of a common-nuclear bis[1.1.1 ]orthocyclophane. First member of a new family of cyclophanes
Woo Young Lee Wonbo Sim and Kwang Do Choi
pg 881; DOI:
10.1039/P19920000881
PDF
Stereoselective syntheses of 2,4:5,6-di-O-isopropylidene-1 -C-phenyl-D-glycero-D-ido-hexitol and 2,4:5,6-di-O-isopropylidene-1 -C-phenyl-D-glycero-D-gulo-hexitol from D-glycero-D-gulo-heptono--lactone. X-Ray structure of 1 -O-acetyl-2,4:5,6-di-O-isopropylidene-1-C-phenyl-D-glycero-D-ido-hexitol
Tony K. M. Shing Hon-Chung Tsui Zhao-Hui Zhou and Thomas C. W. Mak
pg 887; DOI:
10.1039/P19920000887
PDF
Acyliminium ion cyclisations to pyrrolo- and pyrido-[1,2-f]phenanthridine and benzo[de]pyrrolo[2,1-a]isoquinoline ring systems
Gregory J. Hitchings Michael D. Thomas and John M. Vernon
pg 895; DOI:
10.1039/P19920000895
PDF
Novel route to 4,5,6,7-tetrahydroindoles and pyrroles
Takehiko Nishio Norikazu Okuda and Choji Kashima
pg 899; DOI:
10.1039/P19920000899
PDF
Studies in the synthesis of polycyclopentanoids: synthesis, oxa-di--methane rearrangement of annulated bicyclo[2.2.2]octenones and cyclopropane ring cleavage of tetracyclo[6.3.0.0.0]undecenones
Vishwakarma K. Singh Pradeep T. Deota and Ashutosh V. Bedekar
pg 903; DOI:
10.1039/P19920000903
PDF
(Z)-N3-(2-amino-1,2-dicyanovinyl)formamidrazone: a precursor in the synthesis of 1,5-diaminoimidazoles and 6-carbamoyl-1,2-dihydropurines
M. José Alves Brian L. Booth A. Paula Freitas and M. Fernanda J. R. P. Proença
pg 913; DOI:
10.1039/P19920000913
PDF
Reaction of N-substituted cyclic amines with 2,4-dichloroquinazoline, 2,4-dichloropyrimidine, and its 5-methyl derivative
Kenji Yoshida and Masahiro Taguchi
pg 919; DOI:
10.1039/P19920000919
PDF
Total synthesis of fluorinated analogues of inositol and inositol 1,4,5-trisphosphate
Deborah A. Sawyer and Barry V. L. Potter
pg 923; DOI:
10.1039/P19920000923
PDF
Conference dairy

pg 933; DOI:
10.1039/P19920000933
PDF

Issue 8


Front cover

pg X029; DOI:
10.1039/P199200FX029
PDF
Back cover

pg X031; DOI:
10.1039/P199200BX031
PDF
Contents pages

pg P039; DOI:
10.1039/P199200FP039
PDF
Synthesis of axial dialkoxy phosphorus(V)porphyrin derivatives—novel hypervalent phosphorus compounds
Hiroshi Segawa Kazuhiko Kunimoto Akio Nakamoto and Takeo Shimidzu
pg 939; DOI:
10.1039/P19920000939
PDF
Asymmetric Diels–Alder reactions of a chiral sugar nitroalkene: diastereofacial selectivity and regioselectivity
José A. Serrano Luis E. Cáceres and Emilio Román
pg 941; DOI:
10.1039/P19920000941
PDF
Selective photodimerisations of coumarin in crystalline inclusion compounds
Koichi Tanaka and Fumio Toda
pg 943; DOI:
10.1039/P19920000943
PDF
Unsaturated sulfoxides in organic synthesis: a new general furan synthesis
Wing Hong Chan Albert W. M. Lee and Eddy T. T. Chan
pg 945; DOI:
10.1039/P19920000945
PDF
Hydrolytic resolution of tertiary acetylenic acetate esters with the lipase from Candida cylindracea
David O'Hagan and Naveed A. Zaidi
pg 947; DOI:
10.1039/P19920000947
PDF
Synthesis and tritium radiolabelling of fluorinated analogues of myo-inositol
John L. Offer H. Paul Voorheis James C. Metcalfe and Gerry A. Smith
pg 953; DOI:
10.1039/P19920000953
PDF
Synthesis of novel 2-oxo-4-thia-1-azabicyclo[3.3.0]oct-7-ene-8-carboxylic acid derivatives
Steven Coulton and Robert Southgate
pg 961; DOI:
10.1039/P19920000961
PDF
Conversion of cholic acids into aza steroids
Jason Hill James K. Sutherland and Patrick Crowley
pg 969; DOI:
10.1039/P19920000969
PDF
Azoles. Part 9. Synthesis of derivatives of thieno[2,3-d]thiazole, 4H-pyrrolo-[2,3-d]thiazole, 2H-pyrazolo[3,4-d]thiazole and isoxazolo[3,4-d]thiazole from thiazolidine-2,4-dione
Salah Athmani Mahmoud F. Farhat and Brian Iddon
pg 973; DOI:
10.1039/P19920000973
PDF
Avermectin–milbemycin synthetic studies. Part 7. An approach to the southern hemisphere of milbemycin 1
Michelle M. Sulikowski Graham E. R. Ellis Davies and Amos B. Smith III
pg 979; DOI:
10.1039/P19920000979
PDF
Radical cyclization of some unsaturated carbohydrate-derived acetals
Nadira Moufid Yves Chapleur and Patrick Mayon
pg 991; DOI:
10.1039/P19920000991
PDF
Radical cyclization of some unsaturated carbohydrate-derived propargyl ethers and acetals
Nadira Moufid Yves Chapleur and Patrick Mayon
pg 999; DOI:
10.1039/P19920000999
PDF
Conjugated azoalkenes. Part 12. Synthesis of new 1-amino-3-cyanopyrrole, 1,2-diaminopyrrole and pyrrolo[2,3-b] pyrrole derivatives by reaction of some conjugated azoalkenes with activated nitriles
Orazio A. Attanasi Lucia De Crescentini Stefania Santeusanio Franco Serra-Zanetti Alexander McKillop and Zhiyuan Liao
pg 1009; DOI:
10.1039/P19920001009
PDF
Synthesis and absolute stereochemistry of the two diastereoisomers of P3-1-(2-nitrophenyl)ethyl adenosine triphosphate (caged ATP)
John E. T. Corrie Gordon P. Reid David R. Trentham Michael B. Hursthouse and Muhammed A. Mazid
pg 1015; DOI:
10.1039/P19920001015
PDF
Rearrangement of 2-azabicyclo[2.2.1]hept-5-en-3-ones: synthesis of cis-3-aminocyclopentane carboxylic acid derivatives
Christopher F. Palmer Keith P. Parry Stanley M. Roberts and Vladimir Sik
pg 1021; DOI:
10.1039/P19920001021
PDF
Regio- and chemo-selective properties of lipase from Candida cylindracea
Giuseppe Pedrocchi-Fantoni and Stefano Servi
pg 1029; DOI:
10.1039/P19920001029
PDF
Synthesis of lactam and ketone precursors of 2,7-substituted octahydro-pyrrolo[1,2-a]pyrazines and octahydro-2H-pyrido[1,2-a]pyrazines
Stefan Van den Branden Frans Compernolle and Georges J. Hoornaert
pg 1035; DOI:
10.1039/P19920001035
PDF
Novel reaction modes of biliverdin-IX: synthesis and structure of bilatriene dimers
Daniel Krois Hanspeter Kählig and Harald Lehner
pg 1043; DOI:
10.1039/P19920001043
PDF
Synthesis and inhibitory properties of (chlorofluoromethyl)--amino acids, a novel class of irreversible inactivators of decarboxylases
D. Schirlin J. B. Ducep S. Baltzer P. Bey F. Piriou J. Wagner J. M. Hornsperger J. G. Heydt M. J. Jung C. Danzin R. Weiss J. Fischer A. Mitschler and A. De Cian
pg 1053; DOI:
10.1039/P19920001053
PDF
Azido-(amino-)furanosyl nucleosides and their phosphoramidates
Darinka Kataleni and Vinko kari
pg 1065; DOI:
10.1039/P19920001065
PDF
Novel synthesis of indans, tetralones, condensed benzocarbocyclic nitriles and condensed pyridine-2(1H)-thiones from the reactions of cycloalkylidene-malononitriles with arylmethylene(cyano)-acetamide and -thioacetamide
Galal Eldin Hamza Elgemeie Ali M. Elzanate and Abdel Kader Mansour
pg 1073; DOI:
10.1039/P19920001073
PDF
Conference diary

pg 1075; DOI:
10.1039/P19920001075
PDF
Report on the Perkin Journals for 1991

pg vb; DOI:
10.1039/P199200000vb
PDF

Issue 9


Front cover

pg X033; DOI:
10.1039/P199200FX033
PDF
Back cover

pg X035; DOI:
10.1039/P199200BX035
PDF
Contents pages

pg P043; DOI:
10.1039/P199200FP043
PDF
Back matter

pg P047; DOI:
10.1039/P199200BP047
PDF
Highly regioselective [2 + 2] photocycloaddition of aromatic aldehydes to acetylfurans
Howard A. J. Carless and A. Frank E. Halfhide
pg 1081; DOI:
10.1039/P19920001081
PDF
Effect of coenzyme analogues on enantioselectivity of alcohol dehydrogenase
Changsheng Zheng and Robert S. Phillips
pg 1083; DOI:
10.1039/P19920001083
PDF
A simple strategy for obtaining both enantiomers from an aldolase reaction: preparation of L- and D-4-hydroxy-2-ketoglutarate
Nicholas C. Floyd Mark H. Liebster and Nicholas J. Turner
pg 1085; DOI:
10.1039/P19920001085
PDF
N-alkenyl nitrone dipolar cycloaddition routes to piperidines and indolizidines. Part 3. Approach to the gephyrotoxin ring system
Andrew B. Holmes Andrew B. Hughes Adrian L. Smith and Simon F. Williams
pg 1089; DOI:
10.1039/P19920001089
PDF
Preparation and [2 + 3] cycloaddition of thienyl isocyanates with trimethylsilyl azide: one-pot synthesis of the thienyltetrazolin-5-ones
Maurizio Toselli and Paolo Zanirato
pg 1101; DOI:
10.1039/P19920001101
PDF
Synthesis, separation and absolute configuration assignment to enantiomers of 1,3-benzodithiole 1-oxide and 2-alkyl-1,3-benzodithiole 1-oxides
Derek R. Boyd Narain D. Sharma James H. Gorman Robert Dunlop John F. Malone R. Austin S. McMordie and Alex F. Drake
pg 1105; DOI:
10.1039/P19920001105
PDF
Mannich/Friedel–Crafts preparations of 1-(arylmethyl)benzotriazoles and synthetic transformations of their lithio derivatives
Alan R. Katritzky Mikhail F. Gordeev John V. Greenhill and Peter J. Steel
pg 1111; DOI:
10.1039/P19920001111
PDF
General synthesis of homochiral trisubstituted -butyrolactones
David Alker D. Neville Jones G. Mark Taylor and William W. Wood
pg 1119; DOI:
10.1039/P19920001119
PDF
Cathodic carbonylation of 1-halogenopentanes
Kunihisa Yoshida Masaru Kobayashi and Sei-ichi Amano
pg 1127; DOI:
10.1039/P19920001127
PDF
Synthesis and absolute configuration of the naturally occurring cyano glucoside simmondsin
Noritaka Chida Ken Yamada and Seiichiro Ogawa
pg 1131; DOI:
10.1039/P19920001131
PDF
Heterocyclic transformations part 4: a facile transformation of 3-alkyl-6-methyl-1,3-oxazine-2,4(3H)-diones to 6-substituted 5-acetyluracils and 6-thioxo-1,3,5-triazine-2,4(1H,3H,5H)-diones
Harjit Singh Pawan Aggarwal and Subodh Kumar
pg 1139; DOI:
10.1039/P19920001139
PDF
Intramolecular photocycloaddition of 4-phenoxybut-1-enes: a convenient access to the 4-oxatricyclo[7.2.0.0]undeca-2,10-diene skeleton
Siham Y. Al-Qaradawi Kevin B. Cosstick and Andrew Gilbert
pg 1145; DOI:
10.1039/P19920001145
PDF
Structure and stereochemistry of three phytotoxins, syringomycin, syringotoxin and syringostatin, produced by pseudomonas syringae pv. syringae
Naoyuka Fukuchi Akira Isogai Jiro Nakayama Seiji Takayama Shuichi Yamashita Kazuo Suyama Jon Y. Takemoto and Akinori Suzuki
pg 1149; DOI:
10.1039/P19920001149
PDF
A chemoenzymatic synthesis of enantiomerically pure (R)- and (S)-2-methyldecan-1-ol
Patrizia Ferraboschi Paride Grisenti Ada Manzocchi and Enzo Santaniello
pg 1159; DOI:
10.1039/P19920001159
PDF
Multiple-column solid-phase glycopeptide synthesis
Stefan Peters Tim Bielfeldt Morten Meldal Klaus Bock and Hans Paulsen
pg 1163; DOI:
10.1039/P19920001163
PDF
Synthesis of C-functionalized trans-cyclohexyldiethylenetriaminepenta-acetic acids for labelling of monoclonal antibodies with the bismuth-212 -particle emitter
Martin W. Brechbiel and Otto A. Gansow
pg 1173; DOI:
10.1039/P19920001173
PDF
Reaction and spectra of [n.2.1](1,2,3)cyclophanes
Akihiko Tsuge Hironobu Nago Shuntaro Mataka and Masashi Tashiro
pg 1179; DOI:
10.1039/P19920001179
PDF
Conference diary

pg 1187; DOI:
10.1039/P19920001187
PDF

Issue 10


Front cover

pg X037; DOI:
10.1039/P199200FX037
PDF
Back cover

pg X039; DOI:
10.1039/P199200BX039
PDF
Contents pages

pg P049; DOI:
10.1039/P199200FP049
PDF
Back matter

pg P053; DOI:
10.1039/P199200BP053
PDF
Catalytic enantioselective conjugate addition of chiral alkoxydimethylcuprate to (E)-cyclopentadec-2-enone
Kazuhiko Tanaka Junichi Matsui Hitomi Suzuki and Akio Watanabe
pg 1193; DOI:
10.1039/P19920001193
PDF
A corticoid synthesis from 9-hydroxyandrost-4-ene-3,17-dione via a steroidal oxazoline
Nicholas I. Carruthers David R. Andrews Sohaila Garshasb and Robert A. Giusto
pg 1195; DOI:
10.1039/P19920001195
PDF
Efficient one-step synthesis of diastereoisomeric cyclic dipeptides from amino acids: three diastereoisomers of cyclo-L-isoleucyl-L-isoleucine
Brandon Cook Roger R. Hill and Graham E. Jeffs
pg 1199; DOI:
10.1039/P19920001199
PDF
Short enantioselective approach to heteroyohimbine alkaloids from meso-bicyclo[3.3.0]octane-3,7-dione: synthesis of methyl 2-epielenolate
John Leonard Dehimi Quali and Shirley K. Rahman
pg 1203; DOI:
10.1039/P19920001203
PDF
Addition reactions of 2-amino-4-methoxypenta-2,4-dienenitrile with electrophiles containing electron-deficient multiple bonds
Yu-Wen Wang Jim-Min Fang Yu-Ker Wang Mei-Huei Wang Teng-Yao Ko and Yie-Jia Cherng
pg 1209; DOI:
10.1039/P19920001209
PDF
Synthetic approaches towards the novel 1,3-dioxo-1,2-dithiolane moiety in the antitumour antibiotic substance leinamycin
Gerald Pattenden and Anthony J. Shuker
pg 1215; DOI:
10.1039/P19920001215
PDF
Reactions of 1-methyl-4-quinolone with 2-lithio-1,3-dithianes
Rosa Griera Lluis Rigat Mercedes Alvarez and John A. Joule
pg 1223; DOI:
10.1039/P19920001223
PDF
Synthesis of 2,9,10-trioxatricyclo[4.3.1.0]decane analogues of resiniferatoxin
Graham C. Bloomfield Timothy J. Ritchie and Roger Wrigglesworth
pg 1229; DOI:
10.1039/P19920001229
PDF
A simple synthesis of anthracyclinones from 2-acetylquinizarin
Khairuzzaman B. Mullah and James K. Sutherland
pg 1237; DOI:
10.1039/P19920001237
PDF
Model studies related to the cofactor of oxomolybdoenzymes. Part 4. Reduction of the pyrazine ring in quinoxalines and pteridines
James R. Russell C. David Garner and John A. Joule
pg 1245; DOI:
10.1039/P19920001245
PDF
Sulfinyl-controlled formation of diastereoisomerically pure tricarbonyl(oxadiene)iron(0) complexes and a diastereoisomerically pure tetracarbonyl(alkene)iron(0) complex
Arthur Ibbotson Ana C. Reduto dos Reis Stephen P. Saberi Alexandra M. Z. Slawin Susan E. Thomas Gary J. Tustin and David J. Williams
pg 1251; DOI:
10.1039/P19920001251
PDF
Synthesis of a thiashikimic acid derivative
David Adam Andrew A. Freer Neil W. Isaacs Gordon W. Kirby Allison Littlejohn and Mohammad S. Rahman
pg 1261; DOI:
10.1039/P19920001261
PDF
Enzymatic kinetic resolution of flavanone and cis-4-acetoxyflavan
Taeko Izumi Toshimi Hino and Akira Kasahara
pg 1265; DOI:
10.1039/P19920001265
PDF
Thermal [2 + 2]cycloaddition of 1,1-dimethoxyalkenes to acetylenic esters
M. Liliana Graziano M. Rosaria Lesce Flavio Cermola and Guido Cimminiello
pg 1269; DOI:
10.1039/P19920001269
PDF
Corrigenda
Piers R. J. Gaffney Lui Changsheng M. Vaman Rao Colin B. Reese John G. Ward Diana I. Ito Shunsuke Izumi Toshifumi Hirata Takayuki Suga A. W. M. Lee W. H. Chan and E. T. T. Chan
pg 1275; DOI:
10.1039/P19920001275
PDF
Conference diary

pg 1277; DOI:
10.1039/P19920001277
PDF

Issue 11


Front cover

pg X041; DOI:
10.1039/P199200FX041
PDF
Back cover

pg X043; DOI:
10.1039/P199200BX043
PDF
Contents pages

pg P055; DOI:
10.1039/P199200FP055
PDF
Back matter

pg P059; DOI:
10.1039/P199200BP059
PDF
An efficient and regioselective preparation of 4-oxyazetidin-2-ones from 4-trimethylsilylazetidin-2-ones by use of anodic oxidation
Kohji Suda Katsumi Hotoda Jun-ichi Watanabe Kei Shiozawa and Tosnikatsu Takanami
pg 1283; DOI:
10.1039/P19920001283
PDF
Simple synthesis of furanoid and dioxabicyclo[3.3.0]octane lignans
Jayati Mitra and Alok K. Mitra
pg 1285; DOI:
10.1039/P19920001285
PDF
Novel selective heterocyclization of the Michael adducts of ene-hydrazines with dimethyl acetylenedicarboxylate
Tetsuo Yamasaki Hirofumi Nakamura Yoshinari Okamoto Tadashi Okawara and Mitsuru Furukawa
pg 1287; DOI:
10.1039/P19920001287
PDF
Niphatesines E–H, new pyridine alkaloids from the Okinawan marine sponge Niphates sp.
Jun'ichi Kobayashi Chun-min Zeng Masami Ishibashi Hideyuki Shigemori Takuma Sasaki and Yuzuru Mikami
pg 1291; DOI:
10.1039/P19920001291
PDF
New synthesis of diarylalkynes from 1-(arylmethyl)benzotriazoles and arylideneamines
Alan R. Katritzky and Mikhail F. Gordeev
pg 1295; DOI:
10.1039/P19920001295
PDF
Latent inhibitors. Part 8. Synthesis and evaluation of some mechanism-based inhibitors of dihydrofolate reductase
John McGill Lilias Rees Colin J. Suckling and Hamish C. S. Wood
pg 1299; DOI:
10.1039/P19920001299
PDF
Olivanic acid analogues. Part 10. X-Ray crystallographic study of the stereochemistry of some 7-heteroatom-substituted 7-acetyl-8-oxo-3-oxa-1-azabicyclo[4.2.0]octane-2-spirocyclohexanes: functional group control of the stereoselectivity of their reduction products using borohydride reagents
John H. Bateson Stephen C. M. Fell Robert Southgate Drake S. Eggleston and Paul W. Baures
pg 1305; DOI:
10.1039/P19920001305
PDF
Macrocyclisations using allylic radical intermediates. A new synthetic approach to natural 14-membered cembranoids
Nicholas J. G. Cox Stuart D. Mills and Gerald Pattenden
pg 1313; DOI:
10.1039/P19920001313
PDF
Total synthesis of the mycotoxin (–)-zearalenone based on macrocyclisation using a cinnamyl radical intermediate
Stephen A. Hitchcock and Gerald Pattenden
pg 1323; DOI:
10.1039/P19920001323
PDF
cis-Dihydrocatechols as precursors to highly oxygenated troponoids: a fully regiocontrolled synthesis of 3,4-dimethoxy--tropolone
Martin G. Banwell Madeline Corbett Maureen F. Mackay and Sharon L. Richards
pg 1329; DOI:
10.1039/P19920001329
PDF
Chemistry of the mycalamides, antiviral and antitumour compounds from a marine sponge. Part 3. Acyl, alkyl and silyl derivatives
Andrew M. Thompson John W. Blunt Murray H. G. Munro Nigel B. Perry and Lewis K. Pannell
pg 1335; DOI:
10.1039/P19920001335
PDF
Synthesis and properties of tetramethyloctadehydrotridecapentadecafulvalene
Hiroyuki Higuchi Keiko Kitamura Jro Ojima Koji Yamamoto and Gaku Yamamoto
pg 1343; DOI:
10.1039/P19920001343
PDF
Arsenic compounds from the kidney of the giant clam Tridacna maxima: isolation and identification of an arsenic-containing nucleoside
Kevin A. Francesconi John S. Edmonds and Robert V. Stick
pg 1349; DOI:
10.1039/P19920001349
PDF
Preparation of ent-gibberellane and 16-epi-ent-gibberellane
Paul Gaskin Jake MacMillan Ian K. Makinson and Christine L. Willis
pg 1359; DOI:
10.1039/P19920001359
PDF
Application of aryllead(IV) derivatives to the preparation of 3-aryl-4-hydroxy-1-benzopyran-2-ones
Derek H. R. Barton Dervilla M. X. Donnelly Jean-Pierre Finet and Patrick J. Guiry
pg 1365; DOI:
10.1039/P19920001365
PDF
Long wavelength photosensitizers related to chlorins and bacteriochlorins for use in photodynamic therapy
Ravindra K. Pandey Fuu-Yau Shiau Kishore Ramachandran Thomas J. Dougherty and Kevin M. Smith
pg 1377; DOI:
10.1039/P19920001377
PDF
Oxidative dealkylation of 4-substituted N,N-dialkylanilines with molecular oxygen in the presence of acetic anhydride promoted by cobalt(II) or copper(I) chloride
Satoru Murata Kaoru Suzuki Akira Tamatani Masahiro Miura and Masakatsu Nomura
pg 1387; DOI:
10.1039/P19920001387
PDF
Use of 1,3-dioxin-4-ones and related compounds in synthesis. Part 37. 5-Trifluoromethyl-1,3-dioxin-4-ones as versatile building blocks for trifluoromethylated aliphatic compounds
Tomoyasu Iwaoka Tomoko Murohashi Nobuya Katagiri Masayuki Sato and Chikara Kaneko
pg 1393; DOI:
10.1039/P19920001393
PDF
Double ring closure of diacetylenic compounds with activated olefins in the presence of a cobalt(0) catalyst
Zhiming Zhou Mirco Costa and Gian Paolo Chiusoli
pg 1399; DOI:
10.1039/P19920001399
PDF
Lewis acid- or base-catalysed double ring closure of diacetylenic compounds with activated olefins
Zhiming Zhou Mirco Costa and Gian Paolo Chiusoli
pg 1407; DOI:
10.1039/P19920001407
PDF
Fully regiocontrolled synthesis of deacetamidoisocolchicine: formal total synthesis of colchicine
Martin G. Banwell John N. Lambert Madeline Corbett Richard J. Greenwood Jacqueline M. Gulbis and Maureen F. Mackay
pg 1415; DOI:
10.1039/P19920001415
PDF
Enantiospecific synthesis of 3-hetero-dideoxy nucleoside analogues as potential anti-HIV agents
Martin F. Jones Stewart A. Noble Colin A. Robertson Richard Storer Rona M. Highcock and R. Brian Lamont
pg 1427; DOI:
10.1039/P19920001427
PDF
Structural elucidation and absolute configuration of novel -agarofuran (epoxyeudesmene) sesquiterpenes from Maytenus magellanica(Celastraceae)
Antonio G. González Mercedes P. Nuñez Angel G. Ravelo José G. Sazatornil Jesús T. Vázquez Isabel L. Bazzocchi Ezequiel Q. Morales and Orlando M. Muñoz
pg 1437; DOI:
10.1039/P19920001437
PDF
Photoinduced electron-transfer perfluoroalkylation of aminopyridines with perfluoroalkyl iodides
Qing-Yun Chen and Zhan-Ting Li
pg 1443; DOI:
10.1039/P19920001443
PDF
Fluorination of trimethylsilyl phosphites and their structural analogues by sulfuryl chloride fluoride: simple preparation of phosphorofluoridates and related compounds, including deoxynucleoside phosphorofluoridates
Wojciech Dbkowski Friedrich Cramer and Jan Michalski
pg 1447; DOI:
10.1039/P19920001447
PDF
Conference diary

pg 1453; DOI:
10.1039/P19920001453
PDF

Issue 12


Front cover

pg X045; DOI:
10.1039/P199200FX045
PDF
Back cover

pg X047; DOI:
10.1039/P199200BX047
PDF
Contents pages

pg P063; DOI:
10.1039/P199200FP063
PDF
Back matter

pg P067; DOI:
10.1039/P199200BP067
PDF
A convenient method for the extrusion of sulfur dioxide from 2,2,5,5-tetrasubstituted 3-sulfolenes
Ta-Shue Chou and Sheng-Yueh Chang
pg 1459; DOI:
10.1039/P19920001459
PDF
Photocyclisation of phenylglyoxylamides as inclusion complexes with an optically active host derived from tartaric acid: delicate dependence on the substituent of the host and glyoxylamide
Fumio Toda Hisakazu Miyamoto and Rikiya Matsukawa
pg 1461; DOI:
10.1039/P19920001461
PDF
Second generation tumour photosensitisers: the synthesis and biological activity of octaalkyl chlorins and bacteriochlorins with graded amphiphilic character
Keith R. Adams the late Morris C. Berenbaum Raymond Bonnett Alexander N. Nizhnik Antonio Salgado and María Asunción Vallés
pg 1465; DOI:
10.1039/P19920001465
PDF
Unusual behaviour of some - and -lactones towards dichloromethylenation using tris(dimethylamino)phosphine–tetrachloromethane
Alphonse Bandzouzi Mohammed Lakhrissi and Yves Chapleur
pg 1471; DOI:
10.1039/P19920001471
PDF
Remarkably efficient hydrolysis of a 4-nitrophenyl ester by a catalytic antibody raised to an ammonium hapten
Abedawn I. Khalaf George R. Proctor Colin J. Suckling Laura H. Bence June I. Irvine and William H. Stimson
pg 1475; DOI:
10.1039/P19920001475
PDF
Synthesis and properties of tetrazolium-N-phenacylides. Part 2
Dietrich Moderhack and Dirk-Ottfried Bode
pg 1483; DOI:
10.1039/P19920001483
PDF
Preparation and structural properties of hydroxy- and alkoxy-[2.2.1]metacyclophanes
Akihiko Tsuge Tsuyoshi Sawada Shuntaro Mataka Nobuaki Nishiyama Hirofumi Sakashita and Masashi Tashiro
pg 1489; DOI:
10.1039/P19920001489
PDF
Glyantrypine, a novel anthranilic acid-containing metabolite of Aspergillus clavatus
Julia Penn Peter G. Mantle John N. Bilton and Richard N. Sheppard
pg 1495; DOI:
10.1039/P19920001495
PDF
Biomimetic synthesis of agelasidine A
Yoshiyasu Ichikawa Tikako Kashiwagi and Noriko Urano
pg 1497; DOI:
10.1039/P19920001497
PDF
Heterocyclic mesomeric betaines. Part 6. Synthesis and a cycloaddition of a hetero derivative of the 1-methylenephenalene-3-methide anion
W. David Ollis Stephen P. Stanforth and Barry J. Price
pg 1501; DOI:
10.1039/P19920001501
PDF
Total synthesis of (+)-podocarpic and (+)-lambertic acids
Xiao-Jiang Hao Manabu Node and Kaoru Fuji
pg 1505; DOI:
10.1039/P19920001505
PDF
Reactions of squaric acid with phenylhydrazine: structure and nuclear magnetic resonance spectroscopy of cyclobutanetetraone poly(phenylhydrazones)
Hassan S. El Khadem M. Ashraf Shalaby Bruce Coxon and Alexander J. Fatiadi
pg 1511; DOI:
10.1039/P19920001511
PDF
Structures of - and -turmerone
Bernard T. Golding and Esteban Pombo-Villar
pg 1519; DOI:
10.1039/P19920001519
PDF
Asymmetric synthesis of phosphorus analogues of dicarboxylic -amino acids
Vadim A. Soloshonok Yuri N. Belokon Nadezhda A. Kuzmina Victor I. Maleev Nataly Yu. Svistunova Vladimir A. Solodenko and Valery P. Kukhar
pg 1525; DOI:
10.1039/P19920001525
PDF
Initiated, tert-butyl hydroperoxide-loaded, low-temperature autoxidation of alkenes: a chemoselective synthesis of allylic hydroperoxides, allowing analysis of the regioselectivity of hydrogen atom abstraction from some unsymmetrically substituted substrates
John L. Courtneidge and Melanie Bush
pg 1531; DOI:
10.1039/P19920001531
PDF
Initiated tert-butyl hydroperoxide-loaded low-temperature autoxidation of alkenes: alternative hydroperoxide syntheses and the preparation of a complete set of reference materials
John L. Courtneidge Melanie Bush and Lay-See Loh
pg 1539; DOI:
10.1039/P19920001539
PDF
Conference diary

pg 1549; DOI:
10.1039/P19920001549
PDF

Issue 13


Front cover

pg X049; DOI:
10.1039/P199200FX049
PDF
Back cover

pg X051; DOI:
10.1039/P199200BX051
PDF
Contents pages

pg P071; DOI:
10.1039/P199200FP071
PDF
Back matter

pg P075; DOI:
10.1039/P199200BP075
PDF
Mycinamicin biosynthesis: intact incorporation of an intermediate by a chain-elongation process in Micromonospora griseorubida
Hideaki Suzuki Satoshi Takenaka Kenji Kinoshita Yuji Kogami Tatsuro Fujiwara and Toshiro Morohoshi
pg 1555; DOI:
10.1039/P19920001555
PDF
A short synthesis of karahana ether by a radical cyclisation path
Toshio Honda Masayuki Satoh and Yuji Kobayashi
pg 1557; DOI:
10.1039/P19920001557
PDF
New photochemical cyclisation of 9-(6-anilinohexyl)phenanthrene
Akira Sugimoto Ryoichi Hiraoka Hiroo Inoue and Tomohiro Adachi
pg 1559; DOI:
10.1039/P19920001559
PDF
Selective reduction of carboxylic acids with zinc borohydride in the presence of trifluoroacetic anhydride
Brindaban C. Ranu and Asish R. Das
pg 1561; DOI:
10.1039/P19920001561
PDF
Regiospecific deuteriation of chiral 3-isopropyl-2,5-dimethoxy-3,6-dihydropyrazines in the stereospecific synthesis of -deuteriated -amino acids
Janet E. Rose Paul D. Leeson and David Gani
pg 1563; DOI:
10.1039/P19920001563
PDF
Polyfluoroalkylation of octa-1,7-diene promoted by dichlorobis-(-cyclopentadienyl)titanium and iron powder
Chang-Ming Hu and Yao-Ling Qiu
pg 1569; DOI:
10.1039/P19920001569
PDF
C-nucleoside studies. Part 23. New and more direct synthesis of 3-(-D-xylofuranosyl)pyrazole
J. Grant Buchanan M. Luisa Quijano and Richard H. Wightman
pg 1573; DOI:
10.1039/P19920001573
PDF
Olivanic acid analogues. Part 11. Ozonolysis of -ethylideneazetidinones: ozonide fragmentation to -amino acid-N-carboxyanhydrides
John H. Bateson Stephen C. M. Fell Arun C. Kaura and Robert Southgate
pg 1577; DOI:
10.1039/P19920001577
PDF
Reactions of 19-ethoxycarbonyl-19-demethylvincadifformine: synthesis of 19-ethoxycarbonyl-19-demethylapovincamine
Abdelhamid Belattar and J. Edwin Saxton
pg 1583; DOI:
10.1039/P19920001583
PDF
A simple approach to the bicyclo[5.3.1]undecane system present in taxanes
Goutam Saha Atashi Karpha Supti Saha Roy and Subrata Ghosh
pg 1587; DOI:
10.1039/P19920001587
PDF
Synthesis and reactions of some new heterocyclic bismuth-(III) and -(V) compounds. 5,10-Dihydrodibenzo[b,e]bismine and related systems
Hitomi Suzuki Toshihiro Murafuji and Nagao Azuma
pg 1593; DOI:
10.1039/P19920001593
PDF
Oxidation of 1,10-phenanthroline by tetraoxomanganate(VI) and (VII). Preparation, structure and properties of 1H-cyclopenta[2,1-b:3,4-b]dipyridine-2,5-dione
Paul N. W. Baxter Joseph A. Connor John D. Wallis David C. Povey and Anne K. Powell
pg 1601; DOI:
10.1039/P19920001601
PDF
Chemi- and bio-luminescence of coelenterazine analogues with phenyl homologues at the C-2 position
Chen Feng Qi Yasushiro Gomi Takashi Hirano Mamoru Ohashi Yoshihiro Ohmiya and Frederick I. Tsuji
pg 1607; DOI:
10.1039/P19920001607
PDF
Synthesis of 1,2-dihydroisoquinoline-3-carbaldehydes
Gyula Simig
pg 1613; DOI:
10.1039/P19920001613
PDF
Some unexpected reactions involving diphenylketene
Rakesh Maurya Carlos A. Pittol Robert J. Pryce Stanley M. Roberts Russell J. Thomas and Julian O. Williams
pg 1617; DOI:
10.1039/P19920001617
PDF
Synthesis of dendritic polyamides via a convergent growth approach
Kathryn E. Uhrich and Jean M. J. Fréchet
pg 1623; DOI:
10.1039/P19920001623
PDF
Water-promoted organic synthesis using glyco-organic substrates: the Claisen rearrangement
André Lubineau Jacques Augé Nathalie Bellanger and Sylvie Caillebourdin
pg 1631; DOI:
10.1039/P19920001631
PDF
Stereocontrolled synthesis of (2S,3S,8S,9S,4E,6E)-3-amino-9-methoxy-2,6,8-trimethyl-10-phenyldeca-4,6-dienoic acid (Adda), the amino acid characteristic of microcystins and nodularin
Vlark F. Beatty Clive Jennings-White and Mitchell A. Avery
pg 1637; DOI:
10.1039/P19920001637
PDF
Synthesis of selectively multi-labelled histidines with stable isotopes and chiral synthesis of L-histidine from L-aspartic acid
Takashi Furuta Motofusa Katayama Hiromi Shibasaki and Yasuji Kasuya
pg 1643; DOI:
10.1039/P19920001643
PDF
Biosynthetic studies on the chitinase inhibitor, allosamidin. Origin of the carbon and nitrogen atoms
Ze-Yang Zhou Shohei Sakuda and Yasuhiro Yamada
pg 1649; DOI:
10.1039/P19920001649
PDF
Chemoenzymatic approach to the synthesis of the antiviral agents penciclovir and famciclovir in isotopically chiral [13C] labelled form
John T. Sime Roger D. Barnes Stephen W. Elson Richard L. Jarvest and Kevin J. O'Toole
pg 1653; DOI:
10.1039/P19920001653
PDF
Reaction of diphenyl disulfide with alkynes promoted by di-tert-butyl and dibenzoyl peroxide: a useful synthetic route to 3-(and 2,3-) substituted benzo[b]thiophenes
Luisa Benati Pier Carlo Montevecchi and Piero Spagnolo
pg 1659; DOI:
10.1039/P19920001659
PDF
-Stereospecific hydroboration of 13-epi-pimar-8(14)-enes
Arturo San Feliciano Manuel Medarde Esther Caballero Fernando Tomé and Belén Hebrero
pg 1665; DOI:
10.1039/P19920001665
PDF
Synthesis of isothiocyanato-1-[1-(2-benzo[b]thienyl)cyclohexyl]piperidines, potential irreversible ligands at the dopamine re-uptake site
Brian de Costa Clifford George and Celia Dominguez
pg 1671; DOI:
10.1039/P19920001671
PDF
The absolute stereochemistries of (+)-toddalolactone and its related chiral coumarins from Toddalia asiatica(L.) Lam. (T. aculeata Pers.) and their optical purities
Hisashi Ishii Jun-Ichi Kobayashi Eri Sakurada (nee Kawanabe) and Tsutomu Ishikawa
pg 1681; DOI:
10.1039/P19920001681
PDF
Mechanism and stereochemistry of the enzyme-catalysed formation of a 2,2-dimethylchromene ring from a prenylated phenol: conversion of rot-2-enonic acid into deguelin by deguelin cyclase
Prabha Bhandari Leslie Crombie Mark F. Harper John T. Rossiter Mark Sanders and Donald A. Whiting
pg 1685; DOI:
10.1039/P19920001685
PDF
Solid-phase synthesis and characterization of O-dimannosylated heptadecapeptide analogues of human insulin-like growth factor 1 (IGF-1)
Anita M. Jansson Morten Meldal and Klaus Bock
pg 1699; DOI:
10.1039/P19920001699
PDF
Reactions of diene-conjugated 1,3-dipolar intermediates: the formation of cyclopropa[c]isoquinolines from benzonitrile o-alkenylbenzyl ylides and their rearrangements to benzazepines
Keith R. Motion Ian R. Robertson John T. Sharp and Malcolm D. Walkinshaw
pg 1709; DOI:
10.1039/P19920001709
PDF
Synthesis and stereochemistry of an optically active selenonium ylide. X-Ray molecular structure of (+)Se-{4-[(–)-menthyloxycarbonyl]phenyl}(methyl)-selenonium 4,4-dimethyl-2,6-dioxocyclohexylide
Nobumasa Kamigata Yoshihiro Nakamura Koichi Kikuchi Isao Ikemoto Toshio Shimizu and Haruo Matsuyama
pg 1721; DOI:
10.1039/P19920001721
PDF
Synthesis of 2-alkenylpyrazol-3(2H)-one derivatives under mild conditions
Graziano Baccolini Daniele Evangelist Corrado Rizzoli and Paolo Sgarabotto
pg 1729; DOI:
10.1039/P19920001729
PDF
Epoxidation and Baeyer–Villiger oxidation of -hydroxy--unsaturated ketones on exposure to m-chloroperbenzoic acid
Marioara Mendelovici and Erwin Glotter
pg 1735; DOI:
10.1039/P19920001735
PDF
Conference diary

pg 1741; DOI:
10.1039/P19920001741
PDF

Issue 14


Front cover

pg X053; DOI:
10.1039/P199200FX053
PDF
Back cover

pg X055; DOI:
10.1039/P199200BX055
PDF
Contents pages

pg P079; DOI:
10.1039/P199200FP079
PDF
Back matter

pg P083; DOI:
10.1039/P199200BP083
PDF
New triquinane-based host molecules: binding with diamines
Goverdhan Mehta Chebiyyam Prabhakar Natarajan Padmaja and Mysore A. Viswamitra
pg 1747; DOI:
10.1039/P19920001747
PDF
Enzyme-catalysed hydrolysis of 3,5-cis-diacetoxy-4-trans-benzyloxy-methylcyclopentene and the synthesis of aristeromycin precursors
Darren M. LeGrand and Stanley M. Roberts
pg 1751; DOI:
10.1039/P19920001751
PDF
Methylation of 1,2,3-thiadiazole 5-oximes and 5-N-phenylhydrazones
Gerrit L'abbé Lieve Bastin Wim Dehaen Pieter Delbeke and Suzanne Toppet
pg 1755; DOI:
10.1039/P19920001755
PDF
Lipase catalysis in the optical resolution of 2-amino-1-phenylethanol derivatives
Liisa T. Kanerva Katri Rahiala and Eero Vänttinen
pg 1759; DOI:
10.1039/P19920001759
PDF
Synthetic studies towards paspalicine. Part 2. An alternative approach to the synthesis of the C/D ring system
Simon D. Guile J. Edwin Saxton and Mark Thornton-Pett
pg 1763; DOI:
10.1039/P19920001763
PDF
First synthesis of spiro[benzofuran-2,1-isobenzofuran]-3,3-dione and its X-ray crystal structure
Roy M. Letcher Nai-Chiu Kwok and Kung-Kai Cheung
pg 1769; DOI:
10.1039/P19920001769
PDF
Rearrangements of the C/D ring system of the tetracyclic diterpenoid, aphidicolin
James R. Hanson Peter B. Hitchcock Andrew G. Jarvis and Arnold H. Ratcliffe
pg 1773; DOI:
10.1039/P19920001773
PDF
A new synthetic route to pyrrolo[3,2-b]carbazoles, 1H-benzofuro[3,2-f]indoles and 1H-[1]benzothieno[2,3-f]indoles
Laddawan Chunchatprasert K. R. Nagaraja Rao and Patrick V. R. Shannon
pg 1779; DOI:
10.1039/P19920001779
PDF
Rearrangement approaches to cyclic skeletons. Part 8. Total synthesis of ()-nakafuran-8, a marine metabolite with antifeedant properties, on the basis of bridgehead substitution of a bicyclo[2.2.2]oct-5-en-2-one system
Tadao Uyehara Mika Sugimoto Ichiro Suzuki and Yoshinori Yamamoto
pg 1785; DOI:
10.1039/P19920001785
PDF
Isotopically labelled geometric isomers of vinyl groups: reconstructive synthesis of (Z)- and (E)-[7-2H]rotenone
Leslie Crombie Stephen J. Pegg and Donald A. Whiting
pg 1789; DOI:
10.1039/P19920001789
PDF
Chemistry of O-silylated ketene acetals: an efficient synthesis of carbapenem and 1-methylcarbapenem intermediates
Yasuyuki Kita Norio Shibata Takashi Tohjo and Naoki Yoshida
pg 1795; DOI:
10.1039/P19920001795
PDF
N6-substituent effect on the photooxidation of 2,3-O- isopropylideneadenosines with a pyrimido[5,4-g]pteridinetetraone N-oxide. Chemical evidence for the generation and reactivity of adenosyl cation radicals
Magoichi Sako Toru Makino Yukio Kitade Kosaku Hirota and Yoshifumi Maki
pg 1801; DOI:
10.1039/P19920001801
PDF
Novel maleimide-type acceptors based on annelated 1,4-dithiins
Thomas K. Hansen Sukumar K. Varma Stephen Edge and Adam Charlton
pg 1807; DOI:
10.1039/P19920001807
PDF
Regioselective deacylation of 2,4-diacylaminopyrimidine derivatives by Lewis acids and crystal structures of two products
Roger J. Griffin and Philip R. Lowe
pg 1811; DOI:
10.1039/P19920001811
PDF
Studies on chromone derivatives. A direct and efficient one-pot synthesis of 4-chromone-linked 3-(N-acylamino)azetidin-2-ones from imines and N-acylalanine
Dipak Prajapati Asha R. Mahajan and Jagir S. Sandhu
pg 1821; DOI:
10.1039/P19920001821
PDF
Aminodeoxybestatin and epi-aminodeoxybestatin: stereospecific synthesis and aminopeptidase inhibition
Rosario Herranz Soledad Vinuesa Julia Castro-Pichel Concepción Pérez and M. Teresa García-López
pg 1825; DOI:
10.1039/P19920001825
PDF
Two esters of synadenol, a new lathyrane diterpenoid, from the latex of Synadenium compactum(Euphorbiaceae): a crystal structure analysis
George W. J. Olivier Michael G. Rowan Sarah K. Branch Mary F. Mahon and Kieran C. Molloy
pg 1831; DOI:
10.1039/P19920001831
PDF
Photoinduced molecular transformations. Part 131. Synthesis of 18-norsteroids, deoxofukujusonorone and the related steroids, based on a selective -scission of alkoxyl radicals as the key step
Hiroshi Suginome Yutaka Nakayama and Hisanori Senboku
pg 1837; DOI:
10.1039/P19920001837
PDF
Photoinduced molecular transformations. Part 132. A two-step intramolecular transposition of the 17-acetyl group of pregnan-20-one to C-18 through the formation of cyclobutanols by the reaction of the excited carbonyl, followed by a selective -scission of alkoxyl radicals generated from them
Hiroshi Suginome and Yutaka Nakayama
pg 1843; DOI:
10.1039/P19920001843
PDF
Photoinduced molecular transformations. Part 133. New photoinduced deconjugation of steroidal ,-unsaturated cyclic ketone oxime into the ,-unsaturated isomer involving stereospecific proton transfer
Hiroshi Suginome Takashi Ohki Atsushi Nagaoka and Hisanori Senboku
pg 1849; DOI:
10.1039/P19920001849
PDF
Photosensitized oxidation of furans. Part 16. Selective formation and chemical properties of 3H-1,2-dioxoles: a new class of cyclic peroxides
M. Rosaria Iesce Flavio Cermola M. Liliana Graziano Guido Cimminiello and Rachele Scarpati
pg 1855; DOI:
10.1039/P19920001855
PDF
Cytotoxic hydroxypolygodials. X-Ray molecular structure of (1R,3S,5aS,-9aS,9bR)-1,3,5,5a,6,7,8,9,9a,9b-decahydro-1,3-dimethoxy-6,6,9a-trimethylnaphtho[1,2-c]furan
Takehiko Tozyo Fumio Yasuda Hiroshi Nakai and Haruhiko Tada
pg 1859; DOI:
10.1039/P19920001859
PDF
Conference diary

pg 1867; DOI:
10.1039/P19920001867
PDF

Issue 15


Front cover

pg X057; DOI:
10.1039/P199200FX057
PDF
Back cover

pg X059; DOI:
10.1039/P199200BX059
PDF
Contents pages

pg P089; DOI:
10.1039/P199200FP089
PDF
Back matter

pg P093; DOI:
10.1039/P199200BP093
PDF
A convenient synthesis of galactocerebroside using D-glucosamine as a chiral source of the ceramide moiety
Teiichi Murakami Hiroyuki Minamikawa and Masakatsu Hato
pg 1875; DOI:
10.1039/P19920001875
PDF
Selective para-bromination of phenols via a regenerable polymer-bound tetraalkylammonium tribromide
Keith Smith D. Martin James Ian Matthews and Martin R. Bye
pg 1877; DOI:
10.1039/P19920001877
PDF
1H-tetrazole catalysed reactions of trialkyl phosphites: observation of a five-membered cyclic hydrophosphorane intermediate during the transesterification
Yutaka Watanabe Shin-ichi Maehara and Shoichiro Ozaki
pg 1879; DOI:
10.1039/P19920001879
PDF
Silica gel-supported zinc borohydride. Part 3. Regioselective reductive cleavage of methylenecycloalkane oxides to the less-substituted alcohols
Brindaban C. Ranu and Asish R. Das
pg 1881; DOI:
10.1039/P19920001881
PDF
Efficient synthesis of 3H,5H-pyrrolo[3,2-d]pyrimidin-4-one
Mohamed Brakta and G. Doyle Daves Jr
pg 1883; DOI:
10.1039/P19920001883
PDF
Fluorogenic calix[4]arene
Koji Iwamoto Koji Araki Hiroyuki Fujishima and Seiji Shinkai
pg 1885; DOI:
10.1039/P19920001885
PDF
5-Fluorocyclopentadiene: synthesis and utility
Martin A. McClinton and Vladimir Sik
pg 1891; DOI:
10.1039/P19920001891
PDF
Facile deoxygenation of phenols and enols using sodium borohydride–nickel chloride
Feng Wang Kazuhiro Chiba and Masahiro Tada
pg 1897; DOI:
10.1039/P19920001897
PDF
Ketene S,S-acetals as 1,3-dipolarophiles: application to the synthesis of polyhydroxylated pyrrolidines
William O. Moss Robert H. Bradbury Neil J. Hales and Timothy Gallagher
pg 1901; DOI:
10.1039/P19920001901
PDF
Stereoselective syntheses of (–)-goniotriol and (–)-8-acetylgoniotriol from D-glycero-D-gulo-heptono--lactone
Tony K. M. Shing Zhao-Hui Zhou and Thomas C. W. Mak
pg 1907; DOI:
10.1039/P19920001907
PDF
Electrophilic vinylations by vinyllead triacetates and tribenzoates generated by tin–lead exchange
Christopher J. Parkinson John T. Pinhey and Martin J. Stoermer
pg 1911; DOI:
10.1039/P19920001911
PDF
Reaction of 2,6-disubstituted phenols with vinyllead triacetates and alk-1-ynyllead triacetates: synthesis of 6-vinyl- and 6-alkynyl-cyclohexa-2,4-dienones and crystal structure of 1,3,5,7-tetramethyl-3,5-bis(phenylethynyl)-1,3,4,4a,5,8a-hexahydro-1,4-ethenonaphthalene-2,6-dione
Trevor W. Hambley Rodney J. Holmes Christopher J. Parkinson and John T. Pinhey
pg 1917; DOI:
10.1039/P19920001917
PDF
Phthalimidesulfenyl chloride. Part 4. Addition to acetylenes and synthetic utilization of their adducts
Giuseppe Capozzi Luciano Gori Stefano Menichetti and Cristina Nativi
pg 1923; DOI:
10.1039/P19920001923
PDF
Synthesis of linoleic acid with chiral isotopic labelling at a flanking and a medial allylic methylene: the (8R,9Z,12Z)-[8-2H] and (11R,9Z,12Z)-[11-2H]-stereoisomers, and (Z)-[2,2-2H2]non-3-enal
Leslie Crombie and Andrew D. Heavers
pg 1929; DOI:
10.1039/P19920001929
PDF
Synthesis of aminocyclitol moieties of trehalase inhibitors, trehalostatin and trehazolin. Confirmation of the correct structure of the inhibitor
Seiichiro Ogawa and Chikara Uchida
pg 1939; DOI:
10.1039/P19920001939
PDF
Potential antiviral agents. Stereospecific synthesis of purines and pyrimidines substituted with chiral acyclic chains by sugar-ring opening of -L-arabinopyranosyl nucleosides
Christian Périgaud Gilles Gosselin and Jean-Louis Imbach
pg 1943; DOI:
10.1039/P19920001943
PDF
Deprotonative Friedel–Crafts alkylation of arylsilanes with -chlorosulfides
Hiroyuki Ishibashi Hiroshi Sakashita and Masazumi Ikeda
pg 1953; DOI:
10.1039/P19920001953
PDF
Enantiospecific synthesis of aza-analogues of the N-acetylglucosamine-N-acetylmuramic acid repeating unit in peptidoglycan
Stephen F. Moss and Sarah L. Vallance
pg 1959; DOI:
10.1039/P19920001959
PDF
Electrophile-induced intramolecular cyclization of ortho-(aryloxy)phenylalkynes to dibenz[b,f] oxepines
Tsugio Kitamura Tatsuya Takachi Hironobu Kawasato and Hiroshi Taniguchi
pg 1969; DOI:
10.1039/P19920001969
PDF
A synthesis of ()-demethoxydaunomycinone
Kathryn Carr Neil A. Greener Khairuzzaman B. Mullah Fiona M. Somerville and James K. Sutherland
pg 1975; DOI:
10.1039/P19920001975
PDF
Asymmetric Diels–Alder reactions. Part 6. Regio- and stereo-selective cycloadditions of 5-(2,3,4,6-tetra-O-acetyl--D-glucopyranosyloxy)-1,4-naphthoquinone
Brian Beagley Anthony D. M. Curtis Robin G. Pritchard and Richard J. Stoodley
pg 1981; DOI:
10.1039/P19920001981
PDF
Forskolin and 7-deacetylforskolin: study of the reactivity behaviour towards different phosphorylating agents
Bansi Lal and Ashok Kumar Gangopadhyay
pg 1993; DOI:
10.1039/P19920001993
PDF
Electrodic cleavage of the N–S bond in N-tosylcarboxamides. A new entry to N-unsubstituted lactams
Maria Antonietta Casadei Andreas Gessner Achille Inesi Werner Jugelt and Franco Micheletti Moracci
pg 2001; DOI:
10.1039/P19920002001
PDF
Photochemical synthesis of carbon-14 labelled dibenz[a,h]anthracene
Karl L. Platt and Frans Setiabudi
pg 2005; DOI:
10.1039/P19920002005
PDF
Synthetic ionophores. Part 7. Synthesis and ionophore character of uracil based podands
Subodh Kumar Rummi Saini and Harjit Singh
pg 2011; DOI:
10.1039/P19920002011
PDF
Highly enantioselective synthesis of (–)-chokol A
Toshio Suzuki Hitoshi Tada and Katsuo Unno
pg 2017; DOI:
10.1039/P19920002017
PDF
Unsaturated carbohydrates. Part 31. Trichothecene-related and other branched C-pyranoside compounds
Robert J. Ferrier and Paul M. Petersen
pg 2023; DOI:
10.1039/P19920002023
PDF
Reaction of 2-aminothiazoles with reagents containing a C–halogen and a CO electrophilic centre
Victoria J. Compton G. Denis Meakins and Amanda J. Raybould
pg 2029; DOI:
10.1039/P19920002029
PDF
2-Azabicyclo[4.2.0]octane derivatives: stereoselective photochemical synthesis and chemical reactivity
Giorgio Adembri Donato Donati Stefania Fusi and Fabio Ponticelli
pg 2033; DOI:
10.1039/P19920002033
PDF
Studies on a steroidal plant-growth regulator. Part 26. Stereoselective construction of the brassinolide side-chain: new practical syntheses of brassinolide analogues from hyodeoxycholic acid
Wei-Shan Zhou Liang-Fu Huang Li-Qiang Sun and Xin-Fu Pan
pg 2039; DOI:
10.1039/P19920002039
PDF
Corrigendum
Matthew J. Chinn Gilles Iacazio David G. Spackman Nicholas J. Turner and Stanley M. Roberts
pg 2045; DOI:
10.1039/P19920002045
PDF
Conference diary

pg 2047; DOI:
10.1039/P19920002047
PDF

Issue 16


Front cover

pg X061; DOI:
10.1039/P199200FX061
PDF
Back cover

pg X063; DOI:
10.1039/P199200BX063
PDF
Contents pages

pg P095; DOI:
10.1039/P199200FP095
PDF
Back matter

pg P099; DOI:
10.1039/P199200BP099
PDF
Simple and efficient access to the left-hand segment of azinomycins
Kozo Shishido Tomoki Omodani and Masayuki Shibuya
pg 2053; DOI:
10.1039/P19920002053
PDF
One step synthesis of 3,4-dihydro-2H-1,3-oxazines
Karuppiah Pandiarajan and J. Christopher Newton Benny
pg 2055; DOI:
10.1039/P19920002055
PDF
Isoxazol-5(4H)-ones. X-Ray crystal structures of a 4-hydroxyisoxazol-5(4H)-one and a [4,4-biisoxazole]-5(4H),5(4H)-dione formed by oxygen oxidation of 3-tert-butyl-4-methylisoxazol-5(4H)-one
Lotte Brehm Jørgen S. Johansen and Povl Krogsgaard-Larsen
pg 2059; DOI:
10.1039/P19920002059
PDF
Dithiazoles and related compounds. Part. 4. Preparation of 1,4,2-dithiazolium salts unsubstituted at C-5 including the parent heterocycle, NMR spectroscopic evidence for aromaticity, and some novel reactions
Kwok-Fai Wai and Michael P. Sammes
pg 2065; DOI:
10.1039/P19920002065
PDF
Convenient one-pot synthesis of cyclopropyl sulfones via successive alkylation and cyclization of sulfone-stabilized carbanions
Kazuhiko Tanaka and Hitomi Suzuki
pg 2071; DOI:
10.1039/P19920002071
PDF
Preparation of phosphoglycerides by phosphoramidite chemistry
Christopher McGuigan Michael S. Anson and Bernadette Swords
pg 2075; DOI:
10.1039/P19920002075
PDF
Studies in terpenoid biosynthesis. Part 39. The stereochemistry of the relationship between substrate and oxidant in the hydroxylation of aphidicolin at C-18 by Cephalosporium aphidicola
James R. Hanson Peter B. Hitchcock Andrew G. Jarvis and Arnold H. Ratcliffe
pg 2079; DOI:
10.1039/P19920002079
PDF
Chemo-enzymatic synthesis of a lipid-linked core trisaccharide of N-linked glycoproteins
Sabine L. Flitsch Heather L. Pinches James P. Taylor and Nicholas J. Turner
pg 2087; DOI:
10.1039/P19920002087
PDF
Reaction of dianions of acyclic -enamino ketones with electrophiles. Part 2. Oxiranes: synthesis of - and ?-hydroxy--enamino ketones and of -tetrahydrofurylidene ketones
Giuseppe Bartoli Marcella Bosco Cristina Cimarelli Renato Dalpozzo and Gianni Palmier
pg 2095; DOI:
10.1039/P19920002095
PDF
Autorecycling oxidation of alcohols catalysed by pyridodipyrimidines as an NAD(P)+ model
Tomohisa Nagamatsu Hirotake Yamato Masami Ono Shigeki Takarada and Fumio Yoneda
pg 2101; DOI:
10.1039/P19920002101
PDF
Super-acid catalysed addition of allylsilanes to carbonyl compounds; synthetic and mechanistic aspects
Anthony P. Davis and Marcel Jaspars
pg 2111; DOI:
10.1039/P19920002111
PDF
Synthesis of 9-hydroxyalkyl-substituted purines from the corresponding 4-(C-cyanoformimidoyl)imidazole-5-amines
Brian L. Booth Alice M. Dias and M. Fernanda Proença
pg 2119; DOI:
10.1039/P19920002119
PDF
Thermal rearrangement of alkyl O-vinylcarbohydroximates to 2-alkyloxazoles
Masataka Yokoyama Masakazu Irie Keiko Sujino Tsukusi Kagemoto Hideo Togo and Masuo Funabashi
pg 2127; DOI:
10.1039/P19920002127
PDF
Biomimetic synthesis of theonellin isocyanide
Yoshiyasu Ichikawa
pg 2135; DOI:
10.1039/P19920002135
PDF
Corrigendum
Andrew B. Holmes Andrew B. Hughes Adrian L. Smith and Simon F. Williams
pg 2141; DOI:
10.1039/P19920002141
PDF
Conference diary

pg 2143; DOI:
10.1039/P19920002143
PDF

Issue 17


Front cover

pg X065; DOI:
10.1039/P199200FX065
PDF
Back cover

pg X067; DOI:
10.1039/P199200BX067
PDF
Contents pages

pg P103; DOI:
10.1039/P199200FP103
PDF
Back matter

pg P105; DOI:
10.1039/P199200BP105
PDF
First trapping of 5,5-difluorocyclopentadiene
Martin A. McClinton
pg 2149; DOI:
10.1039/P19920002149
PDF
Fluorinated 1,5-dideoxy-1,5-iminoalditols: synthesis of 1,5,6-trideoxy-6-fluoro-1,5-imino-D-glucitol (1,6-dideoxy-6-fluoronojirimycin) and 1,4,5-trideoxy-4-fluoro-1,5-imino-D-ribitol (1,2,5-trideoxy-2-fluoro-1,5-imino-L-ribitol)
Jie Di Bandaru Rajanikanth and Walter A. Szarek
pg 2151; DOI:
10.1039/P19920002151
PDF
Stereochemically controlled synthesis of unsaturated acids by the coupled Baeyer–Villiger and Horner–Wittig reactions: synthesis of (Z)-oct-6-enoic acid
Daniel Levin and Stuart Warren
pg 2155; DOI:
10.1039/P19920002155
PDF
Substituted tetrahydro imidazo[4,5-d][1,2,3]triazoles and hexahydrobutanoimidazo[4,5-d][1,2,3]triazoles from the reaction of 1,2,3-triazolium-1-imides with aryl isocyanates and isothiocyanates. Azolium 1,3-dipoles
Richard N. Butler and David M. Colleran
pg 2159; DOI:
10.1039/P19920002159
PDF
Nickel(0)-promoted synthesis of tetralin lactones from the co-cyclisation of monoynes and octa-1,7-diynes terminally substituted with ester or amide groups
Parveen Bhatarah and Edward H. Smith
pg 2163; DOI:
10.1039/P19920002163
PDF
Regioselective -alkylation of extended enolates derived from enamines of -keto esters. Studies relating to the synthesis of 2-substituted 2-alkoxycarbonylcycloalkanones
Anne Hodgson Joanne Marshall Peter Hallett and Timothy Gallagher
pg 2169; DOI:
10.1039/P19920002169
PDF
Synthetic studies relevant to biosynthetic research on vitamin B12. Part 10. Construction of the east and west building blocks for synthesis of isobacteriochlorins
Alan R. Battersby Michael H. Block Christopher J. R. Fookes Peter J. Harrison Graeme B. Henderson and Finian J. Leeper
pg 2175; DOI:
10.1039/P19920002175
PDF
Synthetic studies relevant to biosynthetic research on vitamin B12. Part 11. Modification of the east and west building blocks and study of different assembly methods for synthesis of isobacteriochlorins
Alan R. Battersby Michael H. Block Finian J. Leeper and Steven C. Zimmerman
pg 2189; DOI:
10.1039/P19920002189
PDF
Synthesis of analogues of 5-iodo-2-deoxyuridine-5-diphosphate
L. John Jennings Marco Macchia and Ann Parkin
pg 2197; DOI:
10.1039/P19920002197
PDF
Novel immunosuppressive butenamides
Christopher A. Axton Michael E. J. Billingham (the late) Paul M. Bishop Peter T. Gallagher Terence A. Hicks E. Ann Kitchen Graham W. Mullier W. Martin Owton Mark G. Parry Susan Scott and David J. Steggles
pg 2203; DOI:
10.1039/P19920002203
PDF
Generation of eight-pi non-Kekul polyenes from the 2+ 4, diethyl azodicarboxylate + tropone cycloadduct
Richard J. Bushby and Christine Jarecki
pg 2215; DOI:
10.1039/P19920002215
PDF
Synthesis of thiospiroacetals. X-Ray crystal structure determinations for (7RS,11RS)-1,4,8-trioxa-13-thiadispiro[4.1.5.3]pentadecan-11-ol and (4RS,6SR)-4-p-nitrobenzoyloxy-1,7-dithiaspiro[5.5]undecane
Mark S. J. Briggs Madeleine Helliwell David Moorcroft and Eric J. Thomas
pg 2223; DOI:
10.1039/P19920002223
PDF
Simple synthetic route to 4-aminobenzaldehydes from anilines
Brita Liedholm
pg 2235; DOI:
10.1039/P19920002235
PDF
Conference diary

pg 2239; DOI:
10.1039/P19920002239
PDF

Issue 18


Front cover

pg X069; DOI:
10.1039/P199200FX069
PDF
Back cover

pg X071; DOI:
10.1039/P199200BX071
PDF
Contents pages

pg P107; DOI:
10.1039/P199200FP107
PDF
Back matter

pg P111; DOI:
10.1039/P199200BP111
PDF
Enzyme-catalysed hydrolysis of dimethyl 7-hydroxy-3,3-dimethyl-2,4-dioxabicyclo[3.3.0]octane-6,8-dicarboxylate and a novel synthesis of neplanocin A
Edward J. Hutchinson Stanley M. Roberts and Andrew J. Thorpe
pg 2245; DOI:
10.1039/P19920002245
PDF
Formation of new hydroxyselenonio and hydroxyammonio-selenuranes from reaction of Se-oxides of 5H,7H-dibenzo[b,g][1,5]diselenocine and N-methyl-5H,7H-dibenzo[b,g][1,5]selenazocine with silyl triflates
Hisashi Fujihara Yoko Ueno Jer-Jye Chiu and Naomichi Furukawa
pg 2247; DOI:
10.1039/P19920002247
PDF
Preparation of dibenzocyclooctadiene lignans and spirodienones by hypervalent iodine oxidation of phenolic dibenzylbutyrolactones
Andrew Pelter Robert S. Ward and Atef Abd-El-Ghani
pg 2249; DOI:
10.1039/P19920002249
PDF
Resolution of mandelic acids by lipase-catalysed transesterifications in organic media: inversion of enantioselectivity mediated by the acyl donor
Toshifumi Miyazawa Sota Kurita Shinichi Ueji Takashi Yamada and Shigeru Kuwata
pg 2253; DOI:
10.1039/P19920002253
PDF
Synthesis of [3-(phosphonomethoxy)pyrrolidin-1-yl] derivatives of pyrimidines and purines: analogues of 2,3-dideoxynucleotides
Michael R. Harnden Richard L. Jarvest and Martin J. Parratt
pg 2259; DOI:
10.1039/P19920002259
PDF
Intramolecular photocycloaddition of 3-benzyloxyprop-1-enes
David C. Blakemore and Andrew Gilbert
pg 2265; DOI:
10.1039/P19920002265
PDF
Structural revision and synthesis of LL-D253 and related chromanone fungal metabolites
I. Michael Chandler C. Rupert McIntyre and Thomas J. Simpson
pg 2271; DOI:
10.1039/P19920002271
PDF
Biosynthesis of LL-D253, a polyketide chromanone metabolite of Phoma pigmentivora: incorporation of 13C, 2H and 18O labelled precursors
I. Michael Chandler C. Rupert McIntyre and Thomas J. Simpson
pg 2285; DOI:
10.1039/P19920002285
PDF
Substituted 1,4,2-dithiazines: synthesis by ring expansion of 1,3-dithiolium cations, solution redox properties and X-ray crystal structures of a monocyclic and a bicyclic derivative
Martin R. Bryce Gordon R. Davison Andrei S. Batsanov and Judith A. K. Howard
pg 2295; DOI:
10.1039/P19920002295
PDF
Stereospecific phenylthio migrations in the synthesis of spirocyclic lactones and ethers from N-methyl-4-piperidone and quinuclidin-3-one
Iain Coldham and Stuart Warren
pg 2303; DOI:
10.1039/P19920002303
PDF
Finkelstein reaction with aqueous hydrogen halides efficiently catalysed by lipophilic quarternary onium salts
Dario Landini Domenico Albanese Sabrina Mottadelli and Michele Penso
pg 2309; DOI:
10.1039/P19920002309
PDF
Aryloxymethyl radical cyclizations mimicking biological C–C bond formation to methoxy groups
S. Asiah Ahmad-Junan Andrew J. Walkington and Donald A. Whiting
pg 2313; DOI:
10.1039/P19920002313
PDF
Synthesis of 1H-isoindoles by a novel rearrangement of some isoquinolin-4(1H)-ones
Diego Armesto William M. Horspool Maria J. Ortiz and Santiago Romano
pg 2321; DOI:
10.1039/P19920002321
PDF
Chemically efficient aza-di--methane photoreactivity with novel stable derivatives of ,-unsaturated carbonyl compounds
Diego Armesto William M. Horspool Maria J. Mancheño and Maria J. Ortiz
pg 2325; DOI:
10.1039/P19920002325
PDF
N-(2-phenylprop-1-enyl)proline methyl ester: equilibrium between the enamine and the aza methine ylide form
Fulvia Felluga Patrizia Nitti Giuliana Pitacco and Ennio Valentin
pg 2331; DOI:
10.1039/P19920002331
PDF
Resolution of the diols of bicyclo[2.2.1]heptane, bicyclo[2.2.2]octane and bicyclo[3.2.1]octane by enzymic hydrolysis, and their absolute configurations
Koichiro Naemura Nobuo Takahashi Shunsuke Tanaka and Hirotsugu Ida
pg 2337; DOI:
10.1039/P19920002337
PDF
Bioreversible protection for the phospho group: bioactivation of the di(4-acyloxybenzyl) and mono(4-acyloxybenzyl) phosphoesters of methylphosphonate and phosphonoacetate
Anthony G. Mitchell William Thomson Dave Nicholls William J. Irwin and Sally Freeman
pg 2345; DOI:
10.1039/P19920002345
PDF
Ene reactions of indane-1,2,3-trione (a super-enophile) and related vicinal tricarbonyl systems
G. Bryon Gill Muhammad S. Hj. Idris and Kirollos S. Kirollos
pg 2355; DOI:
10.1039/P19920002355
PDF
Oxidative cleavage of indane-1,2,3-trione-ene adducts; a convenient synthesis of allyl and allenyl carboxylic acids
G. Bryon Gill Muhammad S. Hj. Idris and Kirollos S. Kirollos
pg 2367; DOI:
10.1039/P19920002367
PDF
Applications of methylsulfonylsulfene in synthesis. Part 1. Conversion of 3,4-dihydro-2H-pyran into cis-2-(C-substituted)tetrahydropyran-3-sulfonates/sulfinates
Brian Beagley Mark R. James Robin G. Pritchard Clive M. Raynor Christopher Smith and Richard J. Stoodley
pg 2371; DOI:
10.1039/P19920002371
PDF
Synthesis of deoxydinucleoside phosphates containing 4-thio substituted pyrimidine nucleobases
Pascale Clivio Jean-Louis Fourrey Jeannette Gasche and Alain Favre
pg 2383; DOI:
10.1039/P19920002383
PDF
Cycloaddition of nitroso dipolarophiles to thiazolium-4-olates. Part 1. Nitrosobenzene and 1-chloro-1-nitrosocyclohexane
Tuvia Sheradsky and Norbert Itzhak
pg 2389; DOI:
10.1039/P19920002389
PDF
Enzymatic resolution of 1,2-diols: comparison between hydrolysis and transesterification reactions
Aldo Bosetti Daniele Bianchi Pietro Cesti Paolo Golini and Sandro Spezia
pg 2395; DOI:
10.1039/P19920002395
PDF
Formation of five-membered lactams by 5-endo-trigonal radical cyclisations of 2-chloro-N-(cycloalk-1-enyl)acetamides: new synthesis of erythrinane skeleton
Tatsunori Sato Nobuyuki Nakamura Keiko Ikeda Michiyo Okada Hiroyuki Ishibashi and Masazumi Ikeda
pg 2399; DOI:
10.1039/P19920002399
PDF
Synthetic, mechanistic and photochemical studies of phosphate esters of substituted benzoins
John E. T. Corrie and David R. Trentham
pg 2409; DOI:
10.1039/P19920002409
PDF
Synthesis of pseudo-ribofuranoses by stereocontrolled reactions on 4-hydroxycyclopent-2-enylmethanol derivatives
Karoline A. Shoberu and Stanley M. Roberts
pg 2419; DOI:
10.1039/P19920002419
PDF
Solid–liquid phase-transfer catalysis without solvent: selective mono- and di-alkylation of benzyl methyl ketone
Alfonso Aranda Angel Díaz Enrique Díez-Barra Antonio de la Hoz Andrés Moreno and Prado Sánchez-Verdú
pg 2427; DOI:
10.1039/P19920002427
PDF
Synthesis of donor–acceptor molecules bridged by turned oligopeptides and their photo-induced electron-transfer process
Hitoshi Tamiaki and Kazuhiro Maruyama
pg 2431; DOI:
10.1039/P19920002431
PDF
Cycloadditions of indolizine-3-carbonitriles with dimethyl acetylenedicarboxylate: formation of [2.2.3]cyclazines and 1 : 2 adducts
Kiyoshi Matsumoto Takane Uchida Hiroshi Yoshida Mitsuo Toda and Akikazu Kakehi
pg 2437; DOI:
10.1039/P19920002437
PDF
Corrigenda
Harjit Singh Subodh Kumar Anupa Jain Paramjit Singh Changsheng Zheng Robert S. Phillips Alphonse Bandzouzi Mohammed Lakhrissi and Yves Chapleur
pg 2443; DOI:
10.1039/P19920002443
PDF
Conference diary

pg 2445; DOI:
10.1039/P19920002445
PDF

Issue 19


Front cover

pg X073; DOI:
10.1039/P199200FX073
PDF
Back cover

pg X075; DOI:
10.1039/P199200BX075
PDF
Contents pages

pg P113; DOI:
10.1039/P199200FP113
PDF
Back matter

pg P117; DOI:
10.1039/P199200BP117
PDF
A new synthesis of 1-aryl-2-oxoalkylphosphonates from nitroalkenes and diethyl phosphite
Dae Young Kim Kilsung Lee and Dong Young Oh
pg 2451; DOI:
10.1039/P19920002451
PDF
A new synthetic method for oligo(phenylenevinylenes) terminated with porphyrins
Noboru Ono Hiroaki Tomita and Kazuhiro Maruyama
pg 2453; DOI:
10.1039/P19920002453
PDF
Monodispersed dendritic polyesters with removable chain ends: a versatile approach to globular macromolecules with chemically reversible polarities
Craig J. Hawker and Jean M. J. Fréchet
pg 2459; DOI:
10.1039/P19920002459
PDF
An enantiospecific synthesis of allosamizoline
Nigel S. Simpkins Stephen Stokes and Alan J. Whittle
pg 2471; DOI:
10.1039/P19920002471
PDF
Synthesis of -bromo substituted ethyl (10-acetoxyphenanthren-9-yl)acetate and 1-(10-acetoxyphenanthren-9-yl)propan-2-one and their transformation to o-quinone methanides
Demetrios N. Nicolaides Spyros G. Adamopoulos Demetrios A. Lefkaditis and Konstantinos E. Litinas
pg 2479; DOI:
10.1039/P19920002479
PDF
Fluorinated acetylenes. Part 10. Cycloadditions of ,-bis(3,3,3-trifluoropropynyl) benzyl benzoate and 1,1-bis(3,3,3-trifluoropropynyl) ethyl ethanoate with furan and cyclopentadiene
Michael G. Barlow Sabiha Tajammal and Anthony E. Tipping
pg 2485; DOI:
10.1039/P19920002485
PDF
Fungal biosynthesis of 3-nitropropanoic acid
Robert L. Baxter A. Bryan Hanley Henry W.-S. Chan Suzanne L. Greenwood Elaine M. Abbot Ian J. McFarlane and Keith Milne
pg 2495; DOI:
10.1039/P19920002495
PDF
Synthesis of 20- and 20-acetamido, amino, nitro and hydroxy derivatives of 14-hydroxy-5,14-pregnane 3-glycosides: pregnanes that bind to the digitalis receptor
John F. Templeton Yangzhi Ling Talal H. Zeglam Kirk Marat and Frank S. LaBella
pg 2503; DOI:
10.1039/P19920002503
PDF
Synthesis of carbocyclic nucleosides: synthesis of ()-2,2-bis(hydroxymethyl)cyclopropyl nucleosides
Takao Izawa Shigeru Nishiyama Shosuke Yamamura Kuniki Kato and Tomohisa Takita
pg 2519; DOI:
10.1039/P19920002519
PDF
Sulfur-mediated intramolecular double Michael-type reaction: synthesis of trans-hydroindanes and mechanism
Masataka Ihara Shuichi Suzuki Nobuaki Taniguchi Keiichiro Fukumoto and Chizuko Kabuto
pg 2527; DOI:
10.1039/P19920002527
PDF
Conversion of some pyrimidine 2-deoxyribonucleosides into the corresponding 2,3-didehydro-2,3-dideoxynucleosides
Bhalchandra V. Joshi T. Sudhakar Rao and Colin B. Reese
pg 2537; DOI:
10.1039/P19920002537
PDF
Acid-mediated rearrangements of 14,17-ethenoestra-1,3,5(10)-trien-17-ols: synthesis of 14,16-ethano-19-norsteroids
James R. Bull Karl Bischofberger Russell I. Thomson Jan L. M. Dillen and Petrus H. van Rooyen
pg 2545; DOI:
10.1039/P19920002545
PDF
Activation of exocyclic -positions of azole N-oxides by O-silylation
Mikael Begtrup and Per Vedsø
pg 2555; DOI:
10.1039/P19920002555
PDF
Oxidation of flavanones using thallium(III) salts: a new route for the synthesis of flavones and isoflavones
Mahavir S. Khanna Om V. Singh Chandra P. Garg and Ram P. Kapoor
pg 2565; DOI:
10.1039/P19920002565
PDF
Corrigendum
Deborah A. Sawyer and Barry V. L. Potter
pg 2569; DOI:
10.1039/P19920002569
PDF
Conference diary

pg 2571; DOI:
10.1039/P19920002571
PDF

Issue 20


Front cover

pg X077; DOI:
10.1039/P199200FX077
PDF
Back cover

pg X079; DOI:
10.1039/P199200BX079
PDF
Contents pages

pg P121; DOI:
10.1039/P199200FP121
PDF
Back matter

pg P125; DOI:
10.1039/P199200BP125
PDF
Intramolecular trapping of an oxacarbene intermediate in the photochemical ring expansion of a cyclopentanone
Krzysztof Switlak David He and Peter Yates
pg 2579; DOI:
10.1039/P19920002579
PDF
Unsual ?/-regiospecificity of (E/Z)-pentadienyltin in the Lewis acid-promoted reaction with an aldehyde
Yutaka Nishigaichi Manabu Fujimoto and Akio Takuwa
pg 2581; DOI:
10.1039/P19920002581
PDF
Preparation and characterization of a four-coordinated ditellurane stabilized by a transannular tellurium–tellurium bond from 1,5-ditelluracyclooctane: a new multicentre hypervalent species
Hisashi Fujihara Yutaka Takaguchi Takeshi Ninoi Tomoki Erata and Naomichi Furukawa
pg 2583; DOI:
10.1039/P19920002583
PDF
Chemoenzymatic synthesis of carbocyclic oxetanocin-A involving a novel photochemical rearrangement
Ian C. Cotterill and Stanley M. Roberts
pg 2585; DOI:
10.1039/P19920002585
PDF
An intramolecular Diels–Alder approach to phorbols: introduction of an oxygenated diene using a palladium catalysed coupling
Philip C. Bulman Page and David C. Jennens
pg 2587; DOI:
10.1039/P19920002587
PDF
Synthesis of C-glycosyltetrazoles related to 3-deoxy-D-arabino-heptulosonic acid 7-phosphate (DAHP); potential inhibitors of early steps in the shikimate pathway
J. Grant Buchanan Andrew P. W. Clelland Trevor Johnson Robert A. C. Rennie and Richard H. Wightman
pg 2593; DOI:
10.1039/P19920002593
PDF
Enamino ketones as precursors of functionalised 2H-thiopyrans and thiopyrano[2,3-c]- and [3,2-b]-benzothiopyrans
Christopher D. Gabbutt John D. Hepworth and B. Mark Heron
pg 2603; DOI:
10.1039/P19920002603
PDF
Stereo- and regio-chemical control in phenylthio migration around rings of sizes 5–15
Malcolm Hannaby Philip Judson and Stuart Warren
pg 2609; DOI:
10.1039/P19920002609
PDF
2-Amino ketene S,S-acetals as -amino acid homoenolate equivalents. Synthesis of 3-substituted prolines and molecular structure of 2-(N-pivaloylpyrrolidin-2-ylidene)-1,3-dithiane
William O. Moss Annette C. Jones Richard Wisedale Mary F. Mahon Kieran C. Molloy Robert H. Bradbury Neil J. Hales and Timothy Gallagher
pg 2615; DOI:
10.1039/P19920002615
PDF
Radical cyclisation reactions leading to polyhydroxylated cyclopentane derivatives: synthesis of (1R,2R,3S,4R)- and (1S,2S,3R,4S)-4-hydroxyethylcyclopentane-1,2,3-triol
Stanley M. Roberts and Karoline A. Shoberu
pg 2625; DOI:
10.1039/P19920002625
PDF
Synthesis of two 6-fluorocarbocyclic nucleosides and incorporation into short segments of DNA
Andrew N. Payne and Stanley M. Roberts
pg 2633; DOI:
10.1039/P19920002633
PDF
Stereoselective synthesis of plant-growth-regulating steroids: brassinolide, castasterone, and their 24,25-substituted analogues
Masayoshi Tsubuki Katsuyuki Keino and Toshio Honda
pg 2643; DOI:
10.1039/P19920002643
PDF
Lithium ion-selective alkylphosphoric acid armed dibenzo- and benzo-14-crown-4 derivatives
Yoichi Habata Manami Ikeda and Sadatoshi Akabori
pg 2651; DOI:
10.1039/P19920002651
PDF
Synthesis of the novel anti-leukaemic tetrahydrocyclopenta[b]benzofuran, rocaglamide and related synthetic studies
Andrew E. Davey Marcel J. Schaeffer and Richard J. K. Taylor
pg 2657; DOI:
10.1039/P19920002657
PDF
Formal total syntheses of (–)-isoavenaciolide and (–)-ethisolide from L-quebrachitol
Noritaka Chida Takahiko Tobe Masami Suwama Masami Ohtsuka and Seiichiro Ogawa
pg 2667; DOI:
10.1039/P19920002667
PDF
Medium-sized cyclophanes. Part 18. 5-tert-Butyl-8-substituted [2.2]metaparacyclophanes: preparation, X-Ray diffraction studies, and their treatment with Lewis acids in benzene
Takehiko Yamato Jun-ichi Matsumoto Kiwamu Tokuhisa Katsuya Tsuji Kazuaki Suehiro and Masashi Tashiro
pg 2675; DOI:
10.1039/P19920002675
PDF
Synthesis of the algicidal allelochemical from Lemna trisulca(duckweed)
Leslie Crombie and Andrew D. Heavers
pg 2683; DOI:
10.1039/P19920002683
PDF
Photochemical reaction of 2,4-dinitrodiphenylacetamide and related compounds: spectroscopic and chemical identification of intermediates
Elisa Fasani Mariella Mella and Angelo Albini
pg 2689; DOI:
10.1039/P19920002689
PDF
A new efficient method for the preparation of 2-fluoro-N-propylnorapomorphine
Sándor Berényi Sándor Hosztafi and Sándor Makleit
pg 2693; DOI:
10.1039/P19920002693
PDF
The potential of carbocyclic nucleosides for the treatment of AIDS: synthesis of some diphosphorylphosphonates possessing potent activity against HIV-coded reverse transcriptase
Diane M. Coe Stanley M. Roberts and Richard Storer
pg 2695; DOI:
10.1039/P19920002695
PDF
Synthesis of (10R)-hepoxilin B3 methyl ester and (10R)-trioxilin B3 methyl ester
Wen-Lian Wu and Yu-Lin Wu
pg 2705; DOI:
10.1039/P19920002705
PDF
Triazolines. Part 32. Synthesis of 1-alkyl-2-aminobenzimidazoles from 5-amino-1-(2-nitroaryl)-1,2,3-triazolines
Emanuela Erba Giorgio Mai and Donato Pocar
pg 2709; DOI:
10.1039/P19920002709
PDF
Selective synthesis and metallochromic properties of pyrrolylated quinoline-5,8-diones
Katsuhira Yoshida Yasunobu Ueno Masaru Suzuki Yukihiro Yoshida and Yuji Kubo
pg 2713; DOI:
10.1039/P19920002713
PDF
Conference diary

pg 2717; DOI:
10.1039/P19920002717
PDF

Issue 21


Front cover

pg X081; DOI:
10.1039/P199200FX081
PDF
Back cover

pg X083; DOI:
10.1039/P199200BX083
PDF
Contents pages

pg P129; DOI:
10.1039/P199200FP129
PDF
Simple stereospecific syntheses of (E)-1-chloro(or bromo)alk-1-enes from alk-1-ynes via hydroboration
Yuzuru Masuda Masayuki Hoshi and Akira Arase
pg 2725; DOI:
10.1039/P19920002725
PDF
Ring enlargement–cyclopentane annulation via thermal oxy-Cope rearrangement
Selvasekaran Janardhanam and Krishnamoorthy Rajagopalan
pg 2727; DOI:
10.1039/P19920002727
PDF
An improved synthesis of 2-substituted-3-furoic acids leading to an intramolecular Diels–Alder reaction between a dienophile and furan diene both containing an electron withdrawing group
Shuyuan Yu Giovanna Beese and Brian A. Keay
pg 2729; DOI:
10.1039/P19920002729
PDF
Chemistry of insect antifeedants from Azadirachta indica(part 12): use of silicon as a control element in the synthesis of a highly functionalized decalin fragment of azadirachtin
Hartmuth C. Kolb Steven V. Ley Alexandra M. Z. Slawin and David J. Williams
pg 2735; DOI:
10.1039/P19920002735
PDF
Chemistry of insect antifeedants from Azadirachta indica(part 13): on the use of the intramolecular Diels–Alder reaction for the construction of trans-fused hydrobenzofuran fragments for azadirachtin synthesis
Hartmuth C. Kolb Steven V. Ley Richard N. Sheppard Alexandra M. Z. Slawin Stephen C. Smith David J. Williams and Anthony Wood
pg 2763; DOI:
10.1039/P19920002763
PDF
Preparation, structure and addition reactions of 4- and 5-aminoimidazoles
Adnan H. M. Al-Shaar David W. Gilmour David J. Lythgoe Ian McClenaghan and Christopher A. Ramsden
pg 2779; DOI:
10.1039/P19920002779
PDF
The synthesis of heterocycles via addition–elimination reactions of 4- and 5-aminoimidazoles
Adnan H. M. Al-Shaar Robert K. Chambers David W. Gilmour David J. Lythgoe Ian McClenaghan and Christopher A. Ramsden
pg 2789; DOI:
10.1039/P19920002789
PDF
Chemistry of silylketenes: a simple preparation of -silyl--stannylacetic esters and their stereoselective Reformatsky-type reaction with aldehydes or aldimines
Shuji Akai Yasunori Tsuzuki Satoshi Matsuda Shinji Kitagaki and Yasuyuki Kita
pg 2813; DOI:
10.1039/P19920002813
PDF
C-alkylations of indoles and pyrroles with -chloro sulfides on an alumina surface: a short synthesis of dithyreanitrile
Hiroyuki Ishibashi Naoki Mita Naoko Matsuba Tomoko Kubo Mariko Nakanishi and Masazumi Ikeda
pg 2821; DOI:
10.1039/P19920002821
PDF
Chemistry of fruit-flies. Spiroacetal-rich secretions in several Bactrocera species from the South-West Pacific region
Mary T. Fletcher Jacqueline A. Wells Mark F. Jacobs Sabine Krohn William Kitching Richard A. I. Drew Christopher J. Moore and Wittko Francke
pg 2827; DOI:
10.1039/P19920002827
PDF
Palladium-catalysed reaction of aryl-substituted allylic alcohols with zinc enolates of -dicarbonyl compounds in the presence of titanium(IV) isopropoxide
Kenji Itoh Naoki Hamaguchi Masahiro Miura and Masakatsu Nomura
pg 2833; DOI:
10.1039/P19920002833
PDF
Alternatives to -diazo ketones for tandem cyclization–cycloaddition and carbenoid–alkyne metathesis strategies. Novel cyclic enol–ether formation via carbonyl ylide rearrangement reactions
David J. Fairfax David J. Austin Simon L. Xu and Albert Padwa
pg 2837; DOI:
10.1039/P19920002837
PDF
Synthesis and reactivity of 4-acyl-5-hydroxytriazolines resulting from thermal reaction of aryl and tosyl azides with 2-substituted indane-1,3-diones
Luisa Benati Pier Carlo Montevecchi Piero Spagnolo and Elisabetta Foresti
pg 2845; DOI:
10.1039/P19920002845
PDF
Sommelet–Hauser or Stevens rearrangement of 1-methyl-2-(substituted-phenyl)piperazinium 1-methylides. Ring enlargement of piperazines to seven- or nine-membered cyclic amines
Tomoko Kitano Naohiro Shirai Manami Motoi and Yoshiro Sato
pg 2851; DOI:
10.1039/P19920002851
PDF
Use of 1,3-dioxin-4-ones and related compounds in synthesis. Part 39. Enantioselective synthesis of 1,3-dioxin-4-ones having 2,3-dihydroxy- or 2,3,4-trihydroxyalkyl groups at the 6-position: versatile building blocks of polyhydroxylated 4–7 carbon backbones
Yoshiaki Sugita Jun-ichi Sakaki Masayuki Sato and Chikara Kaneko
pg 2855; DOI:
10.1039/P19920002855
PDF
3-tert-Butyldimethylsilyloxymethyl-2-lithio-2-phenylsulfonyloxirane as a glycidyl anion equivalent; preparation of terminal epoxy ketones
Sara F. C. Dunn and Richard F. W. Jackson
pg 2863; DOI:
10.1039/P19920002863
PDF
Photochemical reactions of 9-(-anilinoalkyl)-10-bromophenanthrenes
Akira Sugimoto Ryoichi Hiraoka Noriyuki Fukada Hiromi Kosaka and Hiroo Inoue
pg 2871; DOI:
10.1039/P19920002871
PDF
Benzoquinones and related compounds. Part 6. Addition of benzenesulfinic acid to substituted 1,4-quinones
J. Malcolm Bruce and Paul Lloyd-Williams
pg 2877; DOI:
10.1039/P19920002877
PDF
Lipase-catalysed enantioselective acylation of N-protected or unprotected 2-aminoalkan-1-ols
Susana Fernández Rosario Brieva Francisca Rebolledo and Vicente Gotor
pg 2885; DOI:
10.1039/P19920002885
PDF
Enzymatic regioselective acylation of hexoses and pentoses using oxime esters
Rosalino Pulido Fernando López Ortiz and Vicente Gotor
pg 2891; DOI:
10.1039/P19920002891
PDF
Total synthesis of the second messenger analogue D-myo-inositol 1-phosphorothioate 4,5-bisphosphate: optical resolution of DL-1-O-allyl-2,3,6-tri-O-benzyl-myo-inositol and fluorescent labelling of myo-inositol 1,4,5-trisphosphate
Dethard Lampe Stephen J. Mills and Barry V. L. Potter
pg 2899; DOI:
10.1039/P19920002899
PDF
Synthesis and crystal structure of new tetrathiafulvalene derivatives incorporated into thiacrown ether macrocycles
Tine Jørgensen Berhane Girmay Thomas K. Hansen Jan Becher Allan E. Underhill Michael B. Hursthouse Mary E. Harman and Jeremy D. Kilburn
pg 2907; DOI:
10.1039/P19920002907
PDF
New symmetrical tetrathiafulvalene -donors containing nine- and ten-membered dithiaheterocycles
Jai D. Singh and Harkesh B. Singh
pg 2913; DOI:
10.1039/P19920002913
PDF
Efficient formation of a spirotetrahydrofuran ring by the ionic cyclization of bishomoallyl tertiary alcohols via their hypoiodites
Hiroshi Suginome Hisanori Senboku and Atsuhiko Tsunetoshi
pg 2917; DOI:
10.1039/P19920002917
PDF
14-Hydroxy-10-deacetylbaccatin III, a new taxane from Himalayan yew (Taxus wallichiana Zucc.)
Giovanni Appendino Pierluigi Gariboldi Bruno Gabetta Roberto Pace Ezio Bombardelli and Davide Viterbo
pg 2925; DOI:
10.1039/P19920002925
PDF
Palladium-catalysed alkynyl-dehydroxylation of polyfluorophenols
Qing-Yun Chen and Zhan-Ting Li
pg 2931; DOI:
10.1039/P19920002931
PDF
Isomeric ellipticines. Part 1. Synthesis of two linear isomers of the antitumour alkaloid ellipticine
Giovanni Alunni-Bistocchi Pierluigi Orvietani Olivier Mauffret Saïd El Antri Alain Deroussent Pierre C. Jacquignon Serge Fermandjian Adolfo Ricci and Elie Lescot
pg 2935; DOI:
10.1039/P19920002935
PDF
Lewis acid-promoted hetero Diels–Alder reaction of ,-unsaturated thioketones
Shinichi Motoki Takao Saito Takayuki Karakasa Teruyuki Matsushita and Eiji Furuno
pg 2943; DOI:
10.1039/P19920002943
PDF
Useful approach to find the plausible biosynthetic precursors of secondary metabolites using P-450 inhibitors: postulated intermediates of chaetoglobosin A
Hideaki Oikawa Yasunobu Murakami and Akitami Ichihara
pg 2949; DOI:
10.1039/P19920002949
PDF
Biosynthetic study of chaetoglobosin A: origins of the oxygen and hydrogen atoms, and indirect evidence for biological Diels–Alder reaction
Hideaki Oikawa Yasunobu Murakami and Akitami Ichihara
pg 2955; DOI:
10.1039/P19920002955
PDF
Lignin–feruloyl ester cross-links in grasses. Part 1. Incorporation of feruloyl esters into coniferyl alcohol dehydrogenation polymers
John Ralph Richard F. Helm Stéphane Quideau and Ronald D. Hatfield
pg 2961; DOI:
10.1039/P19920002961
PDF
Lignin–feruloyl ester cross-links in grasses. Part 2. Model compound syntheses
John Ralph Richard F. Helm and Stéphane Quideau
pg 2971; DOI:
10.1039/P19920002971
PDF
Reactions of 3-triphenylphosphoranylidene-[b]fused furan-2(3H)-ones with some salicylaldehydes: new synthesis of 3-(2-hydroxyaryl)-coumarins and coumestans
K. E. Litinas and X. N. Stampelos
pg 2981; DOI:
10.1039/P19920002981
PDF
Acylation of aroyl chlorides via a template Friedel–Crafts process: synthesis of indan-1,3-diones
Giovanni Sartori Franca Bigi Raimondo Maggi Davide Baraldi and Giuseppe Casnati
pg 2985; DOI:
10.1039/P19920002985
PDF
Conference diary

pg 2989; DOI:
10.1039/P19920002989
PDF

Issue 22


Front cover

pg X085; DOI:
10.1039/P199200FX085
PDF
Back cover

pg X087; DOI:
10.1039/P199200BX087
PDF
Contents pages

pg P133; DOI:
10.1039/P199200FP133
PDF
Deprotection of silyl ethers using 2,3-dichloro-5,6-dicyano-p-benzoquinone
Kiyoshi Tanemura Tsuneo Suzuki and Takaaki Horaguchi
pg 2997; DOI:
10.1039/P19920002997
PDF
The synthesis of 4-cyanoprogesterone: a potent inhibitor of the enzyme 5--reductase
Margret Haase-Held Maria Hatzis and John Mann
pg 2999; DOI:
10.1039/P19920002999
PDF
4-(Difluoroiodo)tricyclene, an isolable compound of type RIF2 from an aliphatic iodide
Gregory W. Bradley John H. Holloway Han Joong Koh David G. Morris and Paul G. Watson
pg 3001; DOI:
10.1039/P19920003001
PDF
Synthesis of (t-2-benzyloxymethyl-t-3-hydroxy-r-1-methoxycarbonyl)-tetrahydrofuran from an arabino-lactone triflate with K2CO3–MeOH
Takao Izawa Kumiko Nakayama Shigeru Nishiyama Shosuke Yamamura Kuniki Kato and Tomohisa Takita
pg 3003; DOI:
10.1039/P19920003003
PDF
Alkyl migration in competition with phenylthio migration in the acid-catalysed rearrangement of alcohols
Malcolm Hannaby and Stuart Warren
pg 3007; DOI:
10.1039/P19920003007
PDF
Synthesis of the 5-thiorotenoid system from thiochroman-3-one
Christopher D. Gabbutt John D. Hepworth and B. Mark Heron
pg 3015; DOI:
10.1039/P19920003015
PDF
Oxidation of aphidicolin and its conversion into 19-noraphidicolan-16-ol
John F. Gordon James R. Hanson Andrew G. Jarvis and Arnold H. Ratcliffe
pg 3019; DOI:
10.1039/P19920003019
PDF
A practical synthesis of (+)-muscarine from L-rhamnose
Simon J. Mantell George W. J. Fleet and David Brown
pg 3023; DOI:
10.1039/P19920003023
PDF
One-step synthesis of glycosidic spiroketals from 2,3-epoxybutyl glycoside derivatives
Robert J. Ferrier and David W. Hall
pg 3029; DOI:
10.1039/P19920003029
PDF
Synthesis of azanzone A, a new naturally occurring o-naphthoquinone
Roy M. Letcher and Man-Ching Wong
pg 3035; DOI:
10.1039/P19920003035
PDF
New quaternary Corynanth alkaloid from Lerchea bracteata
Dayar Arbain Nordin H. Lajis Deddi Prima Putra Melvyn V. Sargent Brian W. Skelton and Allan H. White
pg 3039; DOI:
10.1039/P19920003039
PDF
Protection of hydroxy groups by silylation: use in peptide synthesis and as lipophilicity modifiers for peptides
John S. Davies Clement L. Higginbotham E. John Tremeer Charles Brown and Richard C. Treadgold
pg 3043; DOI:
10.1039/P19920003043
PDF
Synthetic ionophores. Part 8. Amide–ether–amine-containing macrocycles: synthesis, transport and binding of metal cations
Subodh Kumar Rajinder Singh and Harjit Singh
pg 3049; DOI:
10.1039/P19920003049
PDF
A novel addition–rearrangement of O-(1-benzotriazolylalkyl)oximes with organolithium reagents. Convenient non-oxidative conversions of aldehydes into amides
Alan R. Katritzky Jinlong Jiang John V. Greenhill and Peter J. Steel
pg 3055; DOI:
10.1039/P19920003055
PDF
Simple and condensed -lactams. Part 14. Anomalous behaviour of 1-(4-methoxyphenyl)-4-(tetrazol-5-ylmethyl)azetidin-2-one towards cerium(IV) ammonium nitrate
József Fetter Ern Keskeny Tibor Czuppon Károly Lempert Mária Kajtár-peredy and József Tamás
pg 3061; DOI:
10.1039/P19920003061
PDF
Synthesis of 4-aminopyrimidines from 1,2,4-oxadiazoles. Part 4. A novel heterocyclic rearrangement: formation of 4-hydroximinohexahydropyrimidines from 3-(2-aminoethyl)-4,5-dihydro-1,2,4-oxadiazoles
Dezsö Korbonits Erzsébet Tóbiás-Héja Kálmán Simon György Krámer and Pál Kolonits
pg 3069; DOI:
10.1039/P19920003069
PDF
Reaction of 4-chlorocoumarin with organometallic reagents. Synthesis of trialkylbenzopyrans, 4-chlorobenzopyrans, 4-alkylcoumarins and o-hydroxyphenylprop-2-ynyl alcohols
Angel Alberola Blanca Calvo Alfonso González Ortega and Rafael Pedrosa
pg 3075; DOI:
10.1039/P19920003075
PDF
Synthesis of 1-fluoro-2-phenylvinyl piperidino ketones
Yanchang Shen and Yuefen Zhou
pg 3081; DOI:
10.1039/P19920003081
PDF
Electrophilic reactions of -amino dienenitriles: regiochemistry and stereoselectivity of trisubstituted pentadienyl anions
Chau-Chen Yang and Jim-Min Fang
pg 3085; DOI:
10.1039/P19920003085
PDF
Structure elucidation of monatin, a high-intensity sweetener isolated from the plant Schlerochiton ilicifolius
Robert Vleggaar Louis G. J. Ackerman and Pieter S. Steyn
pg 3095; DOI:
10.1039/P19920003095
PDF
Conjugated azoalkenes. Part 13. Facile and high-yield synthesis of new 1-amino-3-cyano-2,3-dihydropyrrol-2-ols and 1-amino-3-cyano-1H-pyrrol-2(3H)-ones
Orazio A. Attanasi Lucia De Crescentini Alexander McKillop Stefania Santeusanio and Franco Serra-Zanetti
pg 3099; DOI:
10.1039/P19920003099
PDF
Photoinduced molecular transformations. Part 134. Photoinduced stereospecific addition of methanol to 5-cholest-1-en-3-one oxime and photoinduced deconjugation of its 1-methyl derivative involving stereospecific proton transfer
Hiroshi Suginome Atsushi Nagaoka and Hisanori Senboku
pg 3103; DOI:
10.1039/P19920003103
PDF
Photoinduced molecular transformations. Part 135. New synthesis of taiwanin C and justicidin E based on a radical cascade process involving -scission of alkoxyl radicals generated from 3- and 8-aryl-1-ethyl-1,2-dihydrocyclobuta[b]naphthalen-1-ols prepared by thermolysis of (Z)-tert-butyl 3-amino-3-(bicyclo[4.2.0]octa-1,3,5-trien-7-yl)propenoates
Kazuhiro Kobayashi Yoshikazu Kanno Shinzo Seko and Hiroshi Suginome
pg 3111; DOI:
10.1039/P19920003111
PDF
Photoinduced molecular transformations. Part 136. Reactions of alkoxyl radicals generated from hypoiodites of 3-hydroxy-7-oxo-5-steroids. Synthesis of some functionalized oxasteroids
Hiroshi Suginome and Takahiko Kondoh
pg 3119; DOI:
10.1039/P19920003119
PDF
Molecular receptor design for the complexing of dibutylmalonic acid
M Luisa Mussons César Raposo Josefa Anaya Manuel Grande Joaquín R. Morán and M Cruz Caballero
pg 3125; DOI:
10.1039/P19920003125
PDF
2H-benzimidazoles (isobenzimidazoles). Part 7. A new route to triclabendazole [5-chloro-6-(2,3-dichlorophenoxy)-2-methylthio-1H-benzimidazole] and congeneric benzimidazoles
Brian Iddon Peter Kutschy Andrew G. Robinson Hans Suschitzky Walter Kramer and Franz A. Neugebauer
pg 3129; DOI:
10.1039/P19920003129
PDF
Enantioselective trimethylsilylcyanation of some aldehydes catalysed by titanium alkoxide–chiral dialkyl tartrate complexes
Masahiko Hayashi Tohru Matsuda and Nobuki Oguni
pg 3135; DOI:
10.1039/P19920003135
PDF
Asymmetric microbial reduction of tetralones
Jean-Pierre Bégué Claude Cerceau Anukwadey Dogbeavou Laurence Mathé and Sames Sicsic
pg 3141; DOI:
10.1039/P19920003141
PDF
Corrigenda
Changsheng Zheng Robert S. Phillips Alphonse Bandzouzi Mohammed Lakhrissi Yves Chapleur Roy M. Letcher Nai-Chiu Kwok and Kung-Kai Cheung
pg 3145; DOI:
10.1039/P19920003145
PDF
Conference diary

pg 3147; DOI:
10.1039/P19920003147
PDF

Issue 23


Front cover

pg X089; DOI:
10.1039/P199200FX089
PDF
Back cover

pg X091; DOI:
10.1039/P199200BX091
PDF
Contents pages

pg P137; DOI:
10.1039/P199200FP137
PDF
Back matter

pg P141; DOI:
10.1039/P199200BP141
PDF
A versatile strategy for the derivatisation of the carboxy group of amphotericin B: the preparation of C-16 ketone analogues
Michael J. Driver Alexander R. Greenlees and David T. MacPherson
pg 3155; DOI:
10.1039/P19920003155
PDF
Hydroxy-functionalized conjugated nitroolefins as immediate precursors of spiroketals. A new synthesis of 1,7-dioxaspiro[5.5]undecane and (E)-2-methyl-1,7-dioxaspiro[5.6]dodecane
Roberto Ballini and Marino Petrini
pg 3159; DOI:
10.1039/P19920003159
PDF
A novel, chemoselective, one-pot procedure for the simultaneous denitration–deoxygenation of 2-nitroketones by TsNHNH2–NaBH4
Roberto Ballini Roberto Castagnani and Enrico Marcantoni
pg 3161; DOI:
10.1039/P19920003161
PDF
An expeditious and stereocontrolled preparation of 2-azido-2-deoxy--D-glucopyranose derivatives from D-glucal
Denis Tailler Jean-Claude Jacquinet Anne-Marie Noirot and Jean-Marie Beau
pg 3163; DOI:
10.1039/P19920003163
PDF
Investigations on the Giese reaction carried out with polymer-supported organotin reagents
Catharina Bokelmann Wilhelm P. Neumann and Markus Peterseim
pg 3165; DOI:
10.1039/P19920003165
PDF
Ring expansion by intramolecular acylation of phosphine oxides
Paul Wallace and Stuart Warren
pg 3169; DOI:
10.1039/P19920003169
PDF
Peptides from Australian frogs. Structures of the caerins and caeridin 1 from Litoria splendida
David J. M. Stone Russell J. Waugh John H. Bowie John C. Wallace and Michael J. Tyler
pg 3173; DOI:
10.1039/P19920003173
PDF
Synthesis of amido-ureas and the nature of caracasanamide, the hypotensive principle of Verbesina caracasana
Leslie Crombie and Sandra R. M. Jarrett
pg 3179; DOI:
10.1039/P19920003179
PDF
Rapid synthesis of N,N-disubstituted piperazines. Application to the preparation of No carrier added 1-(4-[18F]fluorophenyl)piperazine and of an [18F]-selective ligand of serotoninergic receptors (5HT2 antagonist)
Michael Collins Marie-Claire Lasne and Louisa Barré
pg 3185; DOI:
10.1039/P19920003185
PDF
The role of free radicals in the decomposition of the phytoalexin desoxyhemigossypol
Robert D. Stipanovic Marshall E. Mace Alois A. Bell and Ross C. Beier
pg 3189; DOI:
10.1039/P19920003189
PDF
Acyl radical cyclizations in synthesis. Part 4. Tandem processes: the 7-endo/5-exo serial cyclization approach to enantiomerically pure bicyclo[5.3.0]decan-2-ones
Duncan Batty and David Crich
pg 3193; DOI:
10.1039/P19920003193
PDF
Acyl radical cyclizations in synthesis. Part 5. Further tandem processes: formation of an -methylenecyclohexanone by a cyclization–fragmentation hydrogen-abstraction sequence
Duncan Batty and David Crich
pg 3205; DOI:
10.1039/P19920003205
PDF
Intramolecular [3 + 2]cycloadditions: synthesis of 1-methylene-2,3,3a,4,5,9b-hexahydro-1H-benz[e]indenes and an unsuccessful approach to ergot alkaloids
Michael P. Collins Michael G. B. Drew John Mann and Harry Finch
pg 3211; DOI:
10.1039/P19920003211
PDF
Counterattack reagent: hexamethyldisilane in a direct synthesis of ketene dithioacetals and 2-trimethylsilyl-1,3-dithiane derivatives from 1,3-dithiane
Jih Ru Hwu Taekyo Lee and Bryant A. Gilbert
pg 3219; DOI:
10.1039/P19920003219
PDF
Precursor route chemistry and electronic properties of poly(p-phenylenevinylene), poly[(2,5-dimethyl-p-phenylene)vinylene] and poly[(2,5-dimethoxy-p-phenylene)vinylene]
Paul L. Burn Donal D. C. Bradley Richard H. Friend David A. Halliday Andrew B. Holmes Roger W. Jackson and Arno Kraft
pg 3225; DOI:
10.1039/P19920003225
PDF
Base-catalysed ring contraction of 6,7-dihydro-1-methyl-1H-1,2,5-triazepines to 2,3-dimethyl-1,2,4-triazines
Shinji Shibamoto
pg 3233; DOI:
10.1039/P19920003233
PDF
Isolation and structure elucidation of novel hypotensive agents, niazinin A, niazinin B, niazimicin and niaziminin A + B from Moringa oleifera: the first naturally occurring thiocarbamates
Shaheen Faizi Bina Shaheen Siddiqui Rubeena Saleem Salimuzzaman Siddiqui Khalid Aftab and Anwar-ul-Hassan Gilani
pg 3237; DOI:
10.1039/P19920003237
PDF
Conference diary

pg 3243; DOI:
10.1039/P19920003243
PDF

Issue 24


Index pages

pg A001; DOI:
10.1039/P199200BA001
PDF
Front cover

pg X093; DOI:
10.1039/P199200FX093
PDF
Back cover

pg X095; DOI:
10.1039/P199200BX095
PDF
Contents pages

pg P143; DOI:
10.1039/P199200FP143
PDF
Synthesis of some stable ozonides with anti-malarial activity
Luiz-Claudio de Almeida Barbosa David Cutler John Mann Geoffrey C. Kirby and David C. Warhurst
pg 3251; DOI:
10.1039/P19920003251
PDF
Efficient NAD+-recycling system for ADH-catalysed oxidation in organic media
Shinobu Itoh Tadashi Terasaka Morio Matsumiya Mitsuo Komatsu and Yoshiki Ohshiro
pg 3253; DOI:
10.1039/P19920003253
PDF
The diastereoselectivity of electrophilic attack on trigonal carbon adjacent to a stereogenic centre: diastereoselective alkylation and protonation of open-chain enolates having a stereogenic centre at the position
Ian Fleming and Jeremy J. Lewis
pg 3257; DOI:
10.1039/P19920003257
PDF
The diastereoselectivity of electrophilic attack on trigonal carbon adjacent to a stereogenic centre: diastereoselective protonation, epoxidation and acylation of allylsilanes
Ian Fleming and Jeremy J. Lewis
pg 3267; DOI:
10.1039/P19920003267
PDF
The diastereoselectivity of electrophilic attack on trigonal carbon adjacent to a stereogenic centre: diastereoselective alkylation and protonation of open-chain enolates having a stereogenic centre carrying a silyl group at the position
Roger A. N. C. Crump Ian Fleming John H. M. Hill David Parker N. Laxma Reddy and David Waterson
pg 3277; DOI:
10.1039/P19920003277
PDF
The diastereoselectivity of electrophilic attack on trigonal carbon adjacent to a stereogenic centre: diastereoselective aldol reactions of open-chain enolates having a stereogenic centre carrying a silyl group at the position
Ian Fleming and Jeremy D. Kilburn
pg 3295; DOI:
10.1039/P19920003295
PDF
The stereochemistry of the reaction of allylsilanes with osmium tetroxide and of the epoxidation and methylenation of allylsilanes
Ian Fleming Nicholas J. Lawrence Achintya K. Sarkar and Andrew P. Thomas
pg 3303; DOI:
10.1039/P19920003303
PDF
The regiochemistry and stereochemistry of the hydroboration of allylsilanes
Ian Fleming and Nicholas J. Lawrence
pg 3309; DOI:
10.1039/P19920003309
PDF
Protodesilylation of allylsilanes for the control of double bond geometry exocyclic to a ring
Ian Fleming and Dick Higgins
pg 3327; DOI:
10.1039/P19920003327
PDF
A regioselective and stereospecific synthesis of allylsilanes from secondary allylic alcohol derivatives
Ian Fleming Dick Higgins Nicholas J. Lawrence and Andrew P. Thomas
pg 3331; DOI:
10.1039/P19920003331
PDF
A regiocontrolled and stereocontrolled synthesis of allylsilanes from -silyl enolates
Ian Fleming Salvador Gil Achintya K. Sarkar and Tibur Schmidlin
pg 3351; DOI:
10.1039/P19920003351
PDF
The diastereoselectivity of electrophilic attack on trigonal carbon adjacent to a stereogenic centre
Ian Fleming
pg 3363; DOI:
10.1039/P19920003363
PDF
Reactions of bromotrifluoromethane and related halides. Part 12. Transformation of disulfides into perfluoroalkyl sulfides in the presence of sulfoxylate anion radical precursors
Jean-Louis Clavel Bernard Langlois Roland Nantermet Marc Tordeux and Claude Wakselman
pg 3371; DOI:
10.1039/P19920003371
PDF
One-pot stereoselective synthesis and structural study of 1-methylthio-2-azabuta-1,3-diene-4-carbonitriles
Antonio Lorente José L. Balcázar and Feliciana Florencio
pg 3377; DOI:
10.1039/P19920003377
PDF
An improved route to 1,2,4-trioxanes using tin(IV) as a hydrogen equivalent
Jiaqiang Cai and Alwyn G. Davies
pg 3383; DOI:
10.1039/P19920003383
PDF
N-arylphthalazinium cations: synthons for biphthalazinylidenes via endocyclic phthalazinium ylide intermediates
Richard N. Butler and Carmel S. Pyne
pg 3387; DOI:
10.1039/P19920003387
PDF
Synthesis of cyclopropa[d]thiazolines by a novel and efficient photochemical rearrangement of 1,3-thiazines
Gareth M. Davies Peter B. Hitchcock Richard W. McCabe and Douglas W. Young
pg 3391; DOI:
10.1039/P19920003391
PDF
Base-catalysed reaction of citronellal with phenols
William S. Murphy Anne Culhane Brian Duffy and Sudersan Man Tuladhar
pg 3397; DOI:
10.1039/P19920003397
PDF
Regioselective Friedel–Crafts acylation of 1,2,3,4-tetrahydroquinoline and related nitrogen heterocycles: effects of NH protective groups and ring size
Yuji Ishihara Toshimasa Tanaka and Giichi Goto
pg 3401; DOI:
10.1039/P19920003401
PDF
Stereochemically controlled synthesis of unsaturated alcohols by the Horner–Wittig reaction
Peter M. Ayrey Michael A. Bolton Antony D. Buss Nicholas Greeves Daniel Levin Paul Wallace and Stuart Warren
pg 3407; DOI:
10.1039/P19920003407
PDF
A stereoselective synthesis of trisubstituted alkenes. Part 1. Nickel-catalysed coupling of Grignard reagents with 5-alkyl-2,3-dihydrofurans
Philip J. Kocieski Martin Pritchard Sjoerd N. Wadman Richard J. Whitby and Clive L. Yeates
pg 3419; DOI:
10.1039/P19920003419
PDF
A stereoselective synthesis of trisubstituted alkenes. Part 2. The nickel-catalysed coupling of Grignard reagents with 6-alkyl-3,4-dihydro-2H-pyrans and acyclic enol ethers
Philip A. Ashworth Nicholas J. Dixon Philip J. Kocieski and Sjoerd N. Wadman
pg 3431; DOI:
10.1039/P19920003431
PDF
The synthesis of pyrido [4,3-b]carbazoles from diphenylamine derivatives: alternative routes to and relay syntheses of ellipticines and olivacines
Robin J. Hall Jeremy Marchant Ana M. F. Oliveira-Campos Maria-João R. P. Queiroz and Patrick V. R. Shannon
pg 3439; DOI:
10.1039/P19920003439
PDF
Corrigendum
Alfonso Aranda Angel Díaz Enrique Díez-Barra Antonio de la Hoz Andrés Moreno and Prado Sánchez-Verdú
pg 3451; DOI:
10.1039/P19920003451
PDF
Conference diary

pg 3453; DOI:
10.1039/P19920003453
PDF